CdS Nanoparticles with a Thermoresponsive Polymer Synthesis and Properties英文文献资料.docVIP

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CdS Nanoparticles with a Thermoresponsive Polymer Synthesis and Properties英文文献资料.doc

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CdS Nanoparticles with a Thermoresponsive Polymer Synthesis and Properties英文文献资料

HindawiPublishingCorporation JournalofNanomaterials Volume2012,ArticleID451506,8pages doi:10.1155/2012/451506 ResearchArticle CdSNanoparticleswithaThermoresponsivePolymer: SynthesisandProperties AslamKhan KingAbdullahInstituteforNanotechnology,KingSaudUniversity,Riyadh11451,SaudiArabia CorrespondenceshouldbeaddressedtoAslamKhan,aslampoly@ Received6February2012;Accepted16April2012 AcademicEditor:AnukornPhuruangrat Copyright?2012AslamKhan.ThisisanopenaccessarticledistributedundertheCreativeCommonsAttributionLicense,which permitsunrestricteduse,distribution,andreproductioninanymedium,providedtheoriginalworkisproperlycited. ThispaperdescribesthesynthesisofthermoresponsivecolloidalnanocompositesbasedonCdSandpoly(N-isopropylacrylamide). TheCdSnanoparticleswerepreparedatroomtemperaturefromcadmiumchlorideandsodiumsul?desaltsinthepresenceofan organicligand,3-mercaptopropionicacid(MPA).Theas-preparedMPA-boundCdSnanoparticleswerestableformorethan30 daysandexhibitedgoodopticalproperties.Thee?ectofvariousratiosofMPA/Cd 2+ andH2O/DMF(dimethylformamide)onthe particlesizeoftheCdSnanoparticleswasinvestigatedusingUV-visabsorptionmeasurements.Transmissionelectronmicroscopy studiesshowedthattheparticlesizeswereapproximately4nmindiameter,whichisconsistentwiththesizeobtainedusingUV-vis spectroscopy.TheCdSnanocompositeshowedatemperature-responsivephenomenonasitstemperatureincreasedfrom20to 45 C. ? 1.Introduction toavoidtheformationofcolloidalsulfurandotherspecies thatresultfromtheinstabilityofNa2Sasaprecursor. Colloidal nanoparticles (NPs) have attracted extensive sci- enti?c and industrial interest as a consequence of their highly size-dependent properties and their unique optical andelectronicfeatures[1–4].Thesepropertieshaveledto thepotentialapplicationofcolloidalNPsinlight-emitting devices[5],photoniccrystals[6],andbiologicallabels[7– 10].CdSnanoparticlesrepresentamaterialthatcanbeboth fabricatedandfunctionalizedwithbiomoleculesinasingle step. Consequently, much e?ort has been devot