修改后 郭姣姣译文 - 中英文对照.docx

HANDONGＵＮＩＶＥＲＳＩＴＹ　ＯＦ　ＴＥＣＨＮＯＬＯＧＹ毕业设计（论文）文 献 翻译材料论文/设计题目：溶胶-凝胶法制备氧化锆/石墨烯混合粉体研究翻译材料题目：溶胶凝胶法利用硼/碳还原反应制备硼化锆粉体翻译类型：英译汉学院：资源与环境工程学院专业：资源循环科学与工程姓名：郭姣姣学号导教师：李双评语：指导教师签名： 20 年 月Zirconium Diboride Powders Synthesized byBoro/Carbothermal ReactionUsing Sol-Gel Technology*Ji Huiming，Fan Hongna，Feng Hongjun，Sun Xiaohong(Key Laboratory for Advanced Ceramics and Machining Technology of Ministry ofEducation,School of Materials Science and Engineering, Tianjin University, Tianjin 300072, China)? Tianjin University and Springer-Verlag Berlin Heidelberg 2015采用溶胶凝胶技术通过硼/碳热还原法合成硼化锆粉体季惠明、范红娜、丰红军、孙晓红（先进陶瓷与机械加工技术教育部重点实验室，School of Materials Science and Engineering, Tianjin University, Tianjin 300072, China材料科学与工程学院，天津大学，天津300072，中国）?天津大学和柏林海德堡施普林格出版社2015AbstractA single phase of zirconium diboride(ZrB2)powder was successfully synthesized by sol-gel method inZr-B-C-O system, using zirconium oxychloride(ZrOCl2·8H2O), nano-scale boron and sucrose(C12H22O11)as thestarting materials and propylene oxide(PO)as complexing agent at a low temperature. Simultaneously, the experimental and theoretical studies of ZrB2 synthesized by boro/carbothermal reduction from novel sol-gel technology werediscussed. The results indicated that the pure rod-like ZrB2 powder without residual ZrO2 phase could be obtained witha B/Zr molar ratio of 3.5 at 1 400℃ in argon atmosphere. Besides, in this study, a kinetic model for the Zr-B-C-O system producing ZrB2 by boro/carbothermal reaction was established based on thermodynamic analysis. It was also observed that, with the increase of reaction temperature, the reaction which produced ZrB2 powders changed from theborothermal reaction to boro/carbothermal reaction in the Zr-B-C-O system.Keywords： zirconium diboride; boro/carbothermal reaction; kinetic model; sol-gel method摘要采用溶胶-凝胶法在锆Zr-B-C-O system, using zirconium oxychloride(ZrOCl2?8H2O), nano-scale boron and sucrose(C12H22O11)as the锆-硼-碳-氧系统，利用氧氯化锆（ZrOCl2·8H2O）、纳米硼和蔗糖（C12H22O11）为 starting materials and