Zeph增敏PAR的纸色谱法测定镍(Ⅱ).pdfVIP

• 44 . Aug.2016 Plating and Finishing Vol. 38 No.8 Serial No.281 doi: 10. 3969/j. issn. 1001-3849.2016.08.011 Zeph 增敏 PAR 的纸色谱法测定镇( 11 ) 高文错，余萍，马慧，郭鹏瑶， 高俊杰 (沈阳理工大学环境与化学工程学院，辽宁沈阳 110159) 摘要:提出了通过纸色谱法测定含媒废水中媒( 11 )的方法。使用十四炕基二甲基爷基氯化铁表面 活性剂增敏PAR 显色剂作为浸泡液制备试纸，考察了试纸使用时的最佳条件，建立了测定媒( 11 ) 的新方法。线性范围为 0.5 -100.0 mglL ，方法用于含媒废水中操( 11 )的测定，结果满意。 关键词:十四炕基二甲基辛基氯化接;增敏PAR; 纸色谱;媒( 11 ) 中图分类号: TG115.32 文献标识码:B Nickel ( n) Chromatography- determining by Zeph Sensitized PAR Test Paper GAO Wenhao , YU Ping , MA Hui , GUO Pengyao , GAO Junjie (School of Environmental and Chemical Engineering , Shenyang Ligong University , Shenyang 110159 , China) Abstract: Nickel( 11) concentration was determined by test paper chromatography method. The test paper was prepared by using tetradecyl dimethyl benzyl ammonium chloride ( Zeph ) surfactant sensi- tized PAR chromogenic agent as soak solution. The best condition of the test paper usage was investi- gated , and a new method of nickel ( 11) determination was established. Linear range was o. 5 - 100. 0 mgl L. This method is used for determining the nickel ( 11 ) concentration in nickel containing waste water with satisfied results. Keyword :Zeph ; sensitized PAR; chromatography of test paper; nickel ( 11 ) 染物。因此，需要在产品生产和废水处理过程中经 引言 常测定含镰废水中镰( 11 )的含量。 镀镰工艺广泛的应用到电镀行业当中[1] ，电镀 目前测定含镰废水中镰( 11 )主要采用光度 法(3] 和原子吸收法等[4] 。纸色谱法[5.6] 凭借其操作 企业在镀镰生产过程中，会产生大量含锦废水(2]