高精度光纤荧光测温法的稳定性研究.pdfVIP

第29卷 第2期 计 量 学 报 Vo1．29．№ 2 2008年 4月 ACTA ME rR0L0GICA SINICA April，2008 高精度光纤荧光测温法的稳定性研究 贾丹平， 林乐乐， 苑玮琦， 林应文 (沈阳工业大学，辽宁 沈阳 110023) 摘要：荧光测温方法的分析通常是基于指数曲线而进行的，实践中发现实际的余辉曲线与指数曲线有差别，是 影响仪器稳定性的关键因素。从荧光发光机理出发，分析了产生非指数的根源，提出了用截断归一法来评价余辉 曲线的非指数性，通过几种代表性的荧光材料的光谱特性和截断归～化分析实验，验证了理论分析的正确性，给出 了改善非指数性的措施。在此措施下使测量系统达到0．1℃的分辨率和±0．2℃的精度，可以现场实时进行校准， 测温探头可以互换，已用于微波加热医学生物研究中。 关键词：计量学；温度测量；荧光；稳定性；归一化 中图分类号：TB942 文献标识码：A 文章编号：1000．1158(2008)02—0129—05 A Study for Stability of High Precision Optical Fiber Fluorescent Temperature Measurement System JIA Dan—ping， LIN Le—le， YUAN Wei—qi， LIN Ying—wen (Shenyang University of Technology，Shenyang，Liaoning 1 10023，China) Abstract：Generally，the theoretical analysis of the fluorescent life time temperature measurement is based on the assumption of the exponential life time characteristic，but in practice，the actual curve of the fluorescent ale differ from exponentia1．This is the key influence on the stability of the high-precision fluorescent measurement system．Th e differences are analyzed base on the theoretical mechanism of fluorescent，and a cutting and normalized method is given to describe the degree of the non-exponent of the actual fluorescent curve defer from the exponential curve．Several kinds of typical fluorescence materials spectrum and its cutting and normalized experiment results verify this theoretical analysis．Some effective measures to improve the non—exponent of the system are taken and are applied to a temperature measurement system based on actual fluorescent curve analysis with resolution 0．1℃． precisions±O．2℃．and real-time calibr