原创力文档binuclear cu(ii) and co(ii) complexes of tridentate heterocyclic shiff base derived from salicylaldehyde with 4-aminoantipyrine双核的铜(ii)和(ii)配合物有三叉的杂环与4-aminoantipyrine shiff基础来源于水杨醛.pdfVIP
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binuclear cu(ii) and co(ii) complexes of tridentate heterocyclic shiff base derived from salicylaldehyde with 4-aminoantipyrine双核的铜(ii)和(ii)配合物有三叉的杂环与4-aminoantipyrine shiff基础来源于水杨醛
Hindawi Publishing Corporation
Bioinorganic Chemistry and Applications
Volume 2012, Article ID 601879, 6 pages
doi:10.1155/2012/601879
Research Article
Binuclear Cu(II) and Co(II) Complexes of Tridentate Heterocyclic
Shiff Base Derived from Salicylaldehyde with 4-Aminoantipyrine
Omar Hamad Shihab Al-Obaidi
Chemistry Department, College of Education for Women, Al-Anbar University, Ramadi, Iraq
Correspondence should be addressed to Omar Hamad Shihab Al-Obaidi, dromaralobaidi@
Received 24 September 2011; Revised 26 December 2011; Accepted 28 December 2011
Academic Editor: Nick Katsaros
Copyright © 2012 Omar Hamad Shihab Al-Obaidi. This is an open access article distributed under the Creative Commons
Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is
properly cited.
New binuclear Co(II) and Co(II) complexes of ONO tridentate heterocyclic Schiff base derived from 4-aminoantipyrine with
salicylaldehyde have been synthesized and characterized on the bases of elemental analysis, UV-Vis., FT-IR, and also by aid of
molar conductivity measurements, magnetic measurements, and melting points. It has been found that the Schiff bases with
Cu(II) or Co(II) ion forming binuclear complexes on (1 : 1) “metal : ligand” stoichiometry. The molar conductance measurements
of the complexes in DMSO correspond to be nonelectrolytic nature for all prepared complexes. Distorted octahedral environment
is suggested for metal complexes. A theoretical treatment of the formation of complexes in the gas phase was studied, and this
was done by using the HyperChem-6 program for the molecular mechanics and semi-empirical calculations. The free ligand and
its complexes have been tested for their antibacterial activities aga
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