determination of x-ray diffraction on the phase transformation of microwave-assisted titanate nanotubes during thermal treatmentx射线衍射测定微波相位变换的钛酸纳米管在热处理.pdfVIP

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determination of x-ray diffraction on the phase transformation of microwave-assisted titanate nanotubes during thermal treatmentx射线衍射测定微波相位变换的钛酸纳米管在热处理.pdf

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determination of x-ray diffraction on the phase transformation of microwave-assisted titanate nanotubes during thermal treatmentx射线衍射测定微波相位变换的钛酸纳米管在热处理

Hindawi Publishing Corporation Journal of Nanomaterials Volume 2010, Article ID 837384, 5 pages doi:10.1155/2010/837384 Research Article Determination of X-Ray Diffraction on the Phase Transformation of Microwave-Assisted Titanate Nanotubes during Thermal Treatment Hsin-Hung Ou, Ching-Hui Liao, and Shang-Lien Lo Research Center for Environmental Pollution Prevention and Control Technology, Graduate Institute of Environmental Engineering, National Taiwan University, 71 Chou-Shan Rd., Taipei 106, Taiwan Correspondence should be addressed to Shang-Lien Lo, sllo@.tw Received 26 November 2009; Revised 20 April 2010; Accepted 21 April 2010 Academic Editor: Renzhi Ma Copyright © 2010 Hsin-Hung Ou et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. Based on the determination of X-ray powder diﬀraction, this study aims to investigate the thermal eﬀect on the phase transformation of microwave-assisted titanate nanotubes (MTNTs). The phase transformation is highly dependent on the intercalating amount of Na(I) within MTNTs and on the heating atmosphere. In other words, the presence of Na(I) favors the transformation of TNTs phase into Na Ti O whereas anatase phase selectively formed in the case of MTNTs with less Na(I) 2 6 13 amount. Furthermore, H2 versus O2 is able to form anatase phase and establish a newly transformation pathway. The photocatalytic ability of the calcined MTNTs was also evaluated based on the observed rate constant of trichloroethylene degradation. In addition to anatase phase, the newly phase including Na T