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reactivity ratios for organotin copolymer systems反应性有机锡共聚物系统的比率
Molecules 2010, 15, 2749-2758; doi:10.3390/molecule
OPEN ACCESS
molecules
ISSN 1420-3049
/journal/molecules
Article
Reactivity Ratios for Organotin Copolymer Systems
Mohamed H. El-Newehy, Salem S. Al-Deyab * and Ali Mohsen Ali Al-Hazmi
Department of Chemistry, College of Science, King Saud University, Riyadh 11451, P.O. Box 2455,
Saudi Arabia; E-Mails: mnewehy@ (M.H.E.); petrochem@.sa (A.M.A.)
* Author to whom correspondence should be addressed; E-Mail: ssdeyab@.sa;
Tel.: +966-1-467-5899; Fax: +966-1-467-5992.
Received: 18 March 2010; in revised form: 12 April 2010 / Accepted: 13 April 2010 /
Published: 15 April 2010
Abstract: Di(tri-n-butyltin) itaconate (DTBTI) and monoethyl tributyltin fumarate
(METBTF) were synthesized as organotin monomers. The organotin monomers were
copolymerized with styrene (ST) and methyl methacrylate (MMA) via a free radical
polymerization technique. The overall conversion was kept low (≤15% wt/wt) for all
studied samples and the copolymer composition was determined from tin analysis. The
synthesized monomers and copolymers were characterized by elemental analysis, 1H- and
13C-NMR, and FTIR spectroscopy.
Keywords: organotin monomers; bis(tri-n-butyltin) oxide; maleate; itaconate; styrene;
methyl methacrylate; reactivity ratio
1. Introduction
Copolymers containing both hydrophilic and hydrophobic segments (amphiphilic polymers) are
draw
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