原创力文档recent applications of the (tms)3sih radical-based reagent最近的应用程序(tms)3硅radical-based试剂.pdfVIP
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recent applications of the (tms)3sih radical-based reagent最近的应用程序(tms)3硅radical-based试剂
Molecules 2012, 17, 527-555; doi:10.3390/molecule
OPEN ACCESS
molecules
ISSN 1420-3049
/journal/molecules
Review
Recent Applications of the (TMS) SiH Radical-Based Reagent
3
Chryssostomos Chatgilialoglu 1,* and Jacques Lalevée 2
1 ISOF, Consiglio Nazionale delle Ricerche, 40129 Bologna, Italy
2 Institut de Science des Matériaux de Mulhouse IS2M, LRC CNRS 7228-ENSCMu-UHA,
15, rue Jean Starcky, 68057 Mulhouse Cedex, France; E-Mail: Jacques.Lalevee@uha.fr
* Author to whom correspondence should be addressed; E-Mail: chrys@r.it;
Tel.: +39-051-639-8309; Fax: +39-051-639-8349.
Received: 29 November 2011; in revised form: 29 December 2011 / Accepted: 2 January 2012 /
Published: 6 January 2012
Abstract: This review article focuses on the recent applications of tris(trimethylsilyl)silane
as a radical-based reagent in organic chemistry. Numerous examples of the successful use
of (TMS) SiH in radical reductions, hydrosilylation and consecutive radical reactions are
3
given. The use of (TMS) SiH allows reactions to be carried out under mild conditions with
3
excellent yields of products and remarkable chemo-, regio-, and stereoselectivity. The
strategic role of (TMS) SiH in polymerization is underlined with emphasis on the
3
photo-induced radical polymerization of olefins and photo-promoted cationic polymerization
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