有机前处理方法总汇（Summary of organic pretreatment methods）.docVIP

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有机前处理方法总汇（Summary of organic pretreatment methods）.doc

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有机前处理方法总汇（Summary of organic pretreatment methods）

有机前处理方法总汇（Summary of organic pretreatment methods） Serial number, standard name, standard number, substitute standard number, date of release, date of implementation 1 organic analytical sample pretreatment methods SL 391 1 2007 2007.08.20 2007.11.20 Solid phase extraction gas chromatography / mass spectrometry (GC / MS) 2 SL 3922007 2007.08.20 2007.11.20 Determination of semi volatile organic pollutants in water Purge and trap gas chromatography / mass spectrometry (GC / MS) 3 SL 393 - 2007 2007.08.20 2007.11.20 Volatile organic compounds in water 4 lead, pot, vanadium, phosphorus and other 34 elements determination, SL, 394--2007, 2007.08.20, 2007.11.20 5 technical specifications for surface water quality assessment SL 395--2007 2007.08.20 2007.11.20 The first part: liquid liquid extraction SL 391 - 2007 1 range This part is applicable to extraction and concentration of insoluble or slightly soluble semi volatile organic compounds in water. 2 methods overview Quantitative transfer of a certain amount of water samples to the sub liquid funnel, adjusted to the required pH value, after the sub methylene chloride extraction, dried thick The solvent is replaced by the solvent extracted from the extract in accordance with the solvent required for the purification and determination. 3 interference cancellation 3.1 solvents, reagents, glass containers and other vessels used for handling samples may cause contamination. The whole process shall be verified in blank Are there any disturbances in the materials used in the inspection, if so, find out the sources of interference and eliminate the pollution. Some 3.2 compounds in alkaline extraction conditions easily decomposed, such as organochlorine pesticides may occur dechlorination, phthalates category Compounds may undergo replacement reactions, and phenolic compounds may react to form tannins. The higher the pH value, the stronger the decomposition reaction, and the extraction time The shorter, the weaker the reaction. 3.