响应曲面法优化超声辅助提取虎杖中白藜芦醇的工艺研究.pdfVIP

第8 卷 第9 期 食品安全质量检测学报 Vol. 8 No. 9 2017 年9 月 Journal of Food Safety and Quality Sep. , 2017 响应曲面法优化超声辅助提取虎杖中白藜芦醇的 工艺研究 曹艳蓉, 赵俊平, 毛彩云, 杨永红, 李满秀* (忻州师范学院化学系, 忻州 034000) 摘 要: 目的 优化虎杖中白藜芦醇的提取工艺。方法 以虎杖为原料, 运用超声辅助提取技术对虎杖中的 白藜芦醇进行提取, 以乙醇溶液为溶剂, 考察溶剂浓度、时间、温度、功率、料液比等因素对提取效果的影响, 在单因素实验的基础上, 通过响应曲面法优化提取工艺。结果 最佳工艺参数为: 乙醇浓度 62.85%, 超声时 间37.92 min, 温度60 ℃, 料液比 1:19.45 (g/mL), 超声功率240 W, 此条件下白藜芦醇的提取得率为4.65% 。 结论 本研究改进白藜芦醇的提取工艺, 缩短提取时间, 提高提取得率, 可为白藜芦醇的提取和开发应用提 供参考。 关键词: 超声辅助提取; 响应曲面法; 白藜芦醇 Optimization of ultrasonic-assisted extraction technology of resveratrol from Polygonum Cuspidatum by response surface methodology * CAO Yan-Rong, ZHAO Jun-Ping, MAO Cai-Yun, YANG Yong-Hong, LI Man-Xiu (Department of Chemistry , Xinzhou Teachers University, Xinzhou 034000, China) ABSTRACT: Objective To optimize the extraction process of resveratrol from Polygonum Cuspidatum . Methods The extraction of resveratrol from Polygonum Cuspidatum was achieved by ultrasound assistance. The effects of solvent concentration, ultrasound treatment time, extraction temperature, ultrasound power and material/liquid ratio on extraction efficiency were investigated using ethanol solution as solvent. On the basis of single-factor experiments, the extraction