日本药典 No3 D-J.pdfVIP

JP XV O‹cial Monographs / Daunorubicin Hydrochloride 553553 area of all peaks other than the peak of dantrolene from the sample solution is not larger than the peak area of dantrolene Dantrolene Sodium Hydrate from the standard solution. Operating conditions— ダントロレンナトリウム水和物 Detector: An ultraviolet absorption photometer (wavelength: 300 nm). Column: A stainless steel column about 4 mm in inside di- ameter and about 15 cm in length, packed with silica gel for liquid chromatography (5 mm in particle diameter). Column temperature: A constant temperature of about 30 C. 9 1 H O: 399.29 Mobile phase: A mixture of hexane, acetic acid (100) and C H N NaO .3 / 2 14 9 4 5 2 Monosodium 3-[5-(4-nitrophenyl)furan-2- ethanol (99.5) (90:10:9). ylmethylene]amino-2,5-dioxo-1,3-imidazolidinate Flow rate: Adjust the ‰ow rate so that the retention time of