工作场所空气中丙酮丁酮甲基异丁酮的TWA测定方法.PDFVIP

　　　2004 12 17 6 　　Ch nese J Ind Med 　Dec 2004, Vol.17 No .6 ·359 · 、、 TWA 1 1 2 2 2 梅　勇, 杨　磊, 袁　鹏, 马晓钟, 许　斌 (1., 　430030;2., 　442000) 　　:　、 、 (TWA) 。　, 、 、 。 , 。　 0.02 ～ 1.0 mg/ml、 0.0 15 ～ 1.5 mg/ml 、 0.025 ～ 1.0 mg/ml。 0.9994 ～0.9998 。20 μg/ml, 15 μg/ml, 25 μg/ml, 3.8%～7.0 %。 100 mg 21.6 mg、 26.9 mg 、 19.8 mg。7 d, 。　, 、 、 。2002 《》 (PC-TWA)、 、 。 :;;;;TWA ;;; :R122.1　　:A 　　:1002-221X(2004)06-0359-04 Study on detection of acetone, methyl ethyl ketone and methyl isobutyl ketone for time weighted average concentration in workplace air 1 1 2 2 2 MEI Yong , YANG Le , YUAN Peng , MA X ao-zhong , XU B n (1.Tongji Medical College, Huazhong University of Science and Technology, Wuhan 　430030, China;2.Institute of OccupationalMedicine, Dongfeng　Auto obile Co., Shiyan　442000, China) Abstract:Objective 　To study a gas chromatograph c (GC)detect ng methods of some ketones such as acetone, methyl ethyl ketone and methy l sobutyl ketone n workplace a r for establ sh ng the r TWA concentrat on n Ch na.Method　Acetone, methyl ethyl ketone and methyl sobutyl ketone were sampled w th charcoal tube, desorbed w th carbon d sulf de, then analyzed w th GC.All the processes were based on the nat onal gu del nes for the determ nat on of tox c substances n workplace a r and the determ nat on and chromatography cond t ons w ere opt m zed, too.Result 　The l near l m ts of the method were:acetone 0.02—1.0 mg/ml, methyl ethyl ketone 0.015—1.5 mg/ml, methyl sobutyl ketone 0.025—1.0 mg/ml;the correlat on coeff c ents ranged from 0.9994 to