挤出成型制备重结晶碳化硅热端材料的研究-材料学专业论文.docxVIP

武汉理T大学硕L学位论文ABSTRACT 武汉理T大学硕L学位论文 ABSTRACT Silicon carbide rod as a conventional electro—heating materials has some disadvantages of big resistance discreteness，bad density,low usage temperature and shoa operating life．These problems restrict the technology development of silicon carbide electro·heating element industry．So it is necessary to grope new preparation technology and probe into crystal property for improving application properties and increasing operating life and developing new style electro—heating element．Currently, with the development of Chinese industry furnace and high temperature technology, the requirement of silicon carbide rod is increased,at the same time the usage temperature，operating life and property need to be heightened． This paper prepared high density SiC body for high performance SiC electro-heating element using the high pure SiC and efficient lubricate and plasticizer． The article mainly researching content including： (1)Thc effect of grain composition on the extrusion of SiC was studied．The optimal grain composition of SiC was obtained； (2)The effect of efficient lubricates and plasticizer on the molding pressure and body’density of extrusion was studied．The appropriate dosage of the plasticizer and lubricate was obtained． (3)The effect of the die’s structure on extrusion was studies．The appropriate die’s parameter which was suitable for extrusion was found． (4)Applying vacuum fumace to sinter SiC body,the optimal sintering temperature was found． (5)The crOSS—section pattern was analyzed through SEM．Crystallization of the fine particle and crystal structure was observed． The better extrusion effect was achieved by using 0．6wt％of polyscrylamide． 1．8wt％of oxidized polyethylene wax 6wt％moisture content of SiC pug．The highest body density(2．5659／cm’)was obtained by applying particle of 800pm，100／Hm，59m． And the proportion ofthe particle was 7．2：1：1．8 respectively． The suitable sintering parameters were：2x l O～Pa of vacuum degree，2400