甘蔗糖蜜澄清处理及处理前后组分分析.docxVIP

甘蔗糖蜜澄清处理及处理前后组分分析王湘茹 甘蔗糖蜜澄清处理及处理前后组分分析 王湘茹 ,于淑娟 (华南理工大学 轻工与食品学院 , 广州 510640) 摘要 :甘蔗糖蜜作为糖厂生产过程中主要的副产品 ,含糖量高 ,且含有多酚和黄酮类等抗氧化性成分 ,可 充分利用研制出高附加值的新产品 。但由于糖蜜成分复杂 ,严重影响糖蜜深加工产品品质 ,因此需要有 针对性地进行澄清处理去除胶体 、杂质 。文章糖蜜澄清处理分为稀释 、絮凝 、酸解等流程 ,通过单因素和 正交实验 ,分析确定各工艺流程的条件 。糖蜜 6 倍稀释 ,添加磷酸和絮凝剂絮凝沉淀 ,经高速离心机离 心分离 ,收集上层清液 。然后在 100 ℃水浴 ,p H 值为 2 的条件下酸解 90 mi n ,使糖蜜中蔗糖尽可能多 地转化为还原糖 。最后 ,测定糖蜜澄清处理前后组分含量变化 ,并采用 GC/ M S 检测分析糖蜜澄清处理 前后挥发性物质组分变化 。 关键词 :甘蔗糖蜜 ;澄清处理 ;组分测定 中图分类号 : TS245 . 1 文献标识码 :B 文章编号 :1000 - 9973 (2010) 02 - 0064 - 05 The p ret re at me nt of suga rc a ne mola s se s a nd a nalysi s o n co mpo ne nt WA N G Xia ng2r u , YU Sh u2j ua n ( Colle ge of L i ght Indu st r y a nd Foo d Scie nce , So ut h Chi na U niver sit y of Tec h nolo gy , Gua ngzho u 510640 ,Chi na) Ab stra ct : Sugarcane molasses was t he byp roduct of t he sugar mill in p rocess. It was an excellent so urce of mineral , and active ingredient s like falco noid as well as polyp henol , which co uld be developed into high2added value p ro duct . However , t he co mpo nent s of molasses were co mplicated , which wo uld hinder t he qualit y of t he p roduct s. Therefore , so me p ret reat ment was needed to get rid of t he colloid and ash f ro m t he molasses. In p resent st udy , single2factor experiment and ort ho go nal experiment were designed to optimize t he p ret reat2 ment of t he molasses. As t he result s showed , t he op timal co nditio n of p ret reat ment o n molasses was as fol2 lows , 6 times dilutio n , adding p ho sp horic acid 250 ×1026 , adjusting p H wit h lime to 7 , mixing floc 5 ×1026 , p ut in t he 85 ℃water bat h for 10 min to p recipitate , t hen , high speed cent rif uge was set to separate imp uri2 ty. The supernatant was collected and was adjusted p H by sulp huric acid to 2 , t hen acidolysis in 100 ℃water bat h for 90 min Finally , GC/ MS was taken to analyze t he difference o n t he co mpo nent of molasses before and af ter p ret reat ment . Ke y wo rds : suga r mola sse s ;p ret re