QuEChERS_超高效液相色谱-电喷雾串联质谱法检测鸡肉中11种激素类药物残留.pdfVIP

5 2 Vol. 5 No. 2 2014 2 Journal of Food Safety and Quality Feb. , 2014 QuEChERS/- 11 1 1 1 1 1 1 1 2* 连英杰 , 林升航 , 曾 琪 , 吴 敏 , 徐敦明 , 林立毅 , 周 昱 , 黄志强 (1. , 361000; 2. , 410004) 摘 要: 目的 4 , 3 , 4 QuEChERS/- (ultra pressure liquid chromatography-tandem mass spectrometry, UPLC-MS/MS)方法 , QuEChERS , phenomenex kinetex , (multiple reaction monitoring, MRM)0.1% 结果 11 , 0.991, 3 84.4%~94.1%, (RSD) 7.5%~12.5%, (LOD, S/N 3)(LOQ, S/N 10)0.37~9.55 μg/kg 1.11~28.65 μg/kg结论 , 关键词: QuEChERS; -; ; ; ; Determination of 11 hormones residues in chicken using QuEChERS sample preparation method with ultra performance liquid chromatography-tandem mass spectrometry 1 1 1 1 1 1 LIAN Ying-Jie , LIN Sheng-Hang , ZENG Qi , WU Min , XU Dun-Ming , LIN Li-Yi , ZHOU Yu1, HUANG Zhi-Qiang2* (1. Xiamen Entry-Exit Inspection and Quarantine Bureau, Xiamen 361000, China; 2. Hunan Academy of Inspection and Quarantine , Changsha 410004, China) ABSTRACT: Objective A multi-residue testing method was developed for the simultaneous determination of 4 androgens, 3 progesterones and 4 glucocorticoids in chicken using QuEChERS sample preparation method with ultra performance liquid chromatogr