沙田柚种子油的超临界CO2萃取工艺探究.pdfVIP

沙田柚种子油的超临界C02萃取工艺研究 钟玲1一，李迎霞“3， 吴燕1一，葛发欢“2J (1．中药提取分离过程现代化国家工程研究中心，广州510240；2广东药学院，广州510006 ★ 3．中山大学，广州510275) 摘要：本文首次研究了沙田柚种子油的超临界CO：萃取工艺。考察了萃取压力、时间、温度及 分离条件对沙田柚种子油收率及酸值的影响。确定了较为适宜的萃取工艺：萃取压力30MPa， 时。同时本文运用GC—MS对超临界coz萃取沙田柚种子油的成分进行了分析，鉴定出7种脂肪 酸成分。与传统溶剂提取法进行了比较，超临界COz萃取所得沙出柚种子油外观更好、收率更 高、酸值更低。 关键词：-沙田柚种子油；超临界COz萃取：C-C-MS：酸值 on ExtractionofSeedOilof and C02 Shati-uyu StudySupercritical The ofTheGC-MS Analysis zhonglin91,2，liyingxial3,wuyanl3,gefahuanl2’3‘ ResearchCenterforModernizationofExtractionand (1．NationalEngineering Separation Process Pharmaceutical ofTCM，Guangzhou510240；2．GuangDong University，Guangzhou 5102752) 510006；3．ZhongshanUniversity，Guangzhou Abstract：Inthe carbondioxideextractionoftheseedoilof paper,theprocessofsupercritical isstudied．Theextraction theinfluenceof tO， separation shati·uyu pressure，period，temperatrureand 6ftheseedoilofthe andthe werediscussed．The quality shati—uyu yields optimaloperation was：extractionat at ofextraction 30MPa,extractiontemperature50℃：separator parameter pressure I I at II at6 II pressure6MPa,separatortemperature50C，separatorpressureMPa，separator 2hours．Theseven were GC·MS． at45℃．extraction temperature period compoundsanalysisedby withtraditional seedoiloft