All grass five kinds of medicinal water extract of 6 Determination of elements in.docVIP

 PAGE \* MERGEFORMAT 7 All grass five kinds of medicinal water extract of 6 Determination of elements in [Abstract] the establishment of flame atomic absorption spectrophotometry Chinese violet, Geranium, money grass, lobelia, dandelion extract of medicinal water content of 6 elements. Methods wet digestion for sample preparation, using air - acetylene flame atomic absorption spectrophotometry to measure the wavelength of copper were 324.8nm, Fe 248.3nm, Zn 213.9nm, manganese 279.5nm, Ca 422.7nm, magnesium 285.2nm, using standard Add method recovery experiments. Results The Chinese violet, Geranium, money grass, lobelia, dandelion water extract of medicinal materials of copper, manganese, iron, zinc, calcium, magnesium, copper and the linear range is 0 ~ 2.0μ g/ml, the relevant coefficient of 0.9990, iron the linear range is 0 ~ 20.0μ g/ml, a correlation coefficient of 0.9996, zinc and the linear range is 0.1 ~ 4.0μ g/ml, a correlation coefficient of 0.9990, manganese and the linear range is 0 ~ 2.5μ g / mL, a correlation coefficient of 0.9991, calcium and the linear range is 0 ~ 50.0μ g/mL, a correlation coefficient of 0.9996, magnesium and the linear range is 0 ~ 1.0μ g/mL, a correlation coefficient of 0.9994, this range a good linear relationship . Copper, iron, zinc, manganese, calcium, magnesium, the average recoveries were 97.9%, 95.5%, 96.3%, 95.5%, 96.8%, 94.9%; RSD were 0.7%, 0.9%, 1.5%, 0.9%, 0.6%, 1.2%. Conclusion The precision of the method is good, accuracy and feasibility. These five kinds of medicinal materials by measuring the water extract of six kinds of elements contents of the medicine and clinical application of the preparation process have a certain significance. [Keywords:] Determination of the whole plant of elements in atomic spectrometry [Abstract] Objective To establish a flame atomic absorption spectrophotometry (FAAS) method for the determination of 6 elements in 5 Chinese herbal medicines. Methods FAAS was applied to the determi