Huang detoxification determination of berberine hydrochloride tablets.docVIP

 PAGE \* MERGEFORMAT 8 Huang detoxification determination of berberine hydrochloride tablets [Abstract] Objective To establish Huang detoxifying tablets for determination of berberine hydrochloride. Methods HPLC method to Diamonsil C18 (4.6 mm × 250 mm, 5 μm) column was used, acetonitrile -0.033 mol / L potassium dihydrogen phosphate solution (30:70) as mobile phase, flow rate: 1.0 mL / min, detection wavelength: 265 nm. Results of berberine in the range of 0.043 2 ~ 0.864 μg sample concentration and peak area within the linear relationship between the repetitive RSD = O.89% (n = 6), the average recovery was 99.64%, RSD = 0.74% (n = 5). Conclusion The method is stable, reliable, sensitive, reproducible, and can be used for detoxification Tablets Huang control. [Keywords:] Huang detoxification tablets hydrochloride, HPLC, determination Abstract: Objective To establish the method to determine the content of berberine in Huangju Detoxication Tablets. Methods HPLC was used with Diamonnsil C18 (4.6 mm × 250 mm, 5 μm) as column, acetonitrile-0.033 mol / L potassium dihydrogen phosphate (30: 70) as mobile phase, detection wavelength was at 265 nm, flow rate was 1.0 mL / min. Results In berberine range of 0.043 2 ~ 0.864 μg, the escope and content of the sample peak area had a good linear relationship, reproducibility of RSD = O.89% (n = 6), and the average recovery rate was 99.64% and RSD = 0.74% (n = 5). Conclusion This method is stable, reliable, with high sensitivity and good reproducibility, and can be used for quality control of Huangju Detoxication Tablets. Keywords:: Huangju Detoxication Tablets, berberine, HPLC, content determination Huang detoxification chip from the cork, wild chrysanthemum, Chinese medicine composed of Houttuynia etc., with heat, dehumidification, detoxification, Tonglin and other effects. For the effective control of product quality, we used HPLC method at the main component of cork Fangzhong Jun drug hydrochloride Bo alka