Modified bad quality standard plot Pills.doc

 PAGE \* MERGEFORMAT 15 Modified bad quality standard plot Pills [Abstract] Objective To establish a rotten plot flavored pills quality standards. Methods of preparation of thin-layer chromatography of the angelica, Evodia, costas and Chuen costas, Atractylodes were qualitatively identified, and using high-performance liquid chromatography of the preparation of the active ingredient emodin Rhubarb, rhubarb phenol content. The results detected in samples can angelica, Evodia, costas and Sichuan costas, the characteristics of Atractylodes spots; Emodin in 0.015 63 ~ 0.390 75 μ g linear relationship within the framework of (r = 0.999 9), the average recovery was 100.0%; chrysophanol 0.034 48 ~ 0.862 μ g in the context of a linear relationship between (r = 1.000 0), the average recovery was 99.8%. Conclusion The method is simple, accurate, reproducible and can control pills flavored rotten product quality. [Keywords:] Modified rotten plot pill; quality standards; Emodin; Chrysophanol; high performance liquid chromatography Abstract: ObjectiveTo establish the quality standard of BaiJiang Tablet.MethodsRadix Aangelicae Ssinensis, Fructus Evodiae, Radix Aucklandiae and Radix Vladimiriae, Rhizoma Atractylodis Macrocephalae were identified by TLC.The contents of chrysophanol and emodin were determined by HPLC.ResultsThe linear range of chrysophanol was 0.015 63 ~ 0.3907 5 μ g, and the average recovery was 100.0%; the linear range of emodin was 0.0344 8 ~ 0.862 μ g, and the average recovery was 99.8%. ConclusionThe method is simple, accurate and with a good reproducibility and may be used for quality control of Jiaweilanji Pill. Keywords:: Jiaweilanji Pill; Quality standard; Chrysophanol and emodin; HPLC Modified rotten plot pills from rhubarb, costas, Sichuan costas, angelica, Atractylodes, Evodia and other traditional Chinese medicine, has a negatively-oriented hysteresis effect, can be used for food accumulation, chest full of swelling of the liver nausea, abdo