原创力文档dispersibility, shape and magnetic properties of nano-fe3o4 particles可分散性、形状和nano-fe3o4粒子的磁性.pdfVIP
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dispersibility, shape and magnetic properties of nano-fe3o4 particles可分散性、形状和nano-fe3o4粒子的磁性
Materials Sciences and Applications, 2011, 2, 1644-1653
doi:10.4236/msa.2011.211219 Published Online November 2011 (http://www.SciRP.org/journal/msa)
Dispersibility, Shape and Magnetic Properties of
Nano-Fe O Particles
3 4
1 2 2 2* 3
Xiaojuan Liang , Haowei Shi , Xiangchen Jia , Yuxiang Yang , Xiangnong Liu
1College of Chemistry and Materials Engineering, Wenzhou University, Wenzhou, China; 2Department of Chemistry, East China
University of Science Technology, Nanjing, China; 3Analysis Test Center, Yangzhou University, Yangzhou, China.
*
Email: yxyang@
Received July 25th, 2010; revised November 19th, 2010; accepted September 8th, 2011.
ABSTRACT
Nano-Fe O particles were prepared by a two-step microemulsion method, the influence of molar ratio of water to
3 4
NP-5 (R), alkali concentration and temperature on dispersibility and shape of the nanoparticles were discussed. Mag-
netic studies were also carried out using VSM in this paper. It was found that the optimum preparation parameters are
R = 6.0, alkali concentration = 2.5 mol·L–1 , initial total iron concentration as 0.88 mol·L–1 , and the temperature being
30˚C, the prepared nano magnetite particles have uniform size and good dispersibility with a crystal structure belong-
ing to cubic Fe O and lattice parameters of a = 8.273 Å. The results of magnetic studies show, magnetic properties of
3 4
particles are influenced by dispersibility of nanoparticles which depends on size of clusters. The better dispersibility of
nanoparticles leads to more ordered inner magnetic vector, and so the stronger magnetic behavior of nano-Fe O par-
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