effect of oxalate precursor formation temperature on magnetic properties of nicuzn ferrites草酸的影响前体的形成温度对磁性nicuzn铁氧体.pdfVIP

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effect of oxalate precursor formation temperature on magnetic properties of nicuzn ferrites草酸的影响前体的形成温度对磁性nicuzn铁氧体.pdf

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effect of oxalate precursor formation temperature on magnetic properties of nicuzn ferrites草酸的影响前体的形成温度对磁性nicuzn铁氧体

Materials Sciences and Application, 2011, 2, 1097-1108 1097 doi:10.4236/msa.2011.28148 Published Online August 2011 (http://www.SciRP.org/journal/msa) Effect of Oxalate Precursor Formation Temperature on Magnetic Properties of NiCuZn Ferrites 1* 1 2 3 3 Neelam S. Shinde , Sujata S. Khot , Bhimrao P. Ladgaonkar , Bharat B. Kale , Sanjay Apte , Prasad 4 4 M. Tamhankar , Shrikant C. Watawe 1Dr.Datar Science, Dr.Behere Arts and Shri. Pilukaka Joshi Commerce (D.B.J.) College, Chiplun, Maharashtra, India; 2Shankarrao Mohite Mahavidhayalaya, Akluj, Solapur, Maharashtra, India; 3Center for Materials for Electronic Technology, Pashan, Pune, India; 4Lokmanya Tilak Institute of Postgraduate Teaching and Research, Gogate Jogalekar College, Ratnagiri, Maharashtra, India. * Email: neelamshinde1976@ st th th Received January 1 , 2011; revised March 10 , 2011; accepted June 13 , 2011. ABSTRACT Ni-Cu-Zn ferrites with general formula Ni Zn Cu Fe O (with x = 0.3, 0.4, 0.5 and 0.6) have been synthesized 0.5 0.5-x/2 x/2 2 4 using oxalate precursor method with different precursor reaction temperatures in the range 10˚C to 70 ˚C. The Curie temperatures obtained using AC susceptibility measurements are found to be in the range 150˚C to 350 ˚C, the meas- urements also show single domain structure for all the samples except few compositions obtained at 35 ˚C precursor reaction temperature, show a multi-domain behaviour. The saturation magnetization is found to be in the range 20 to 51 emu/gm, while the magnetic moment is found to