effect of sintering temperature on structural and magnetic properties of ni0.55zn0.45fe2o4 ferrites烧结温度对结构的影响和ni0.55zn0.45fe2o4磁性铁氧体.pdfVIP

Materials Sciences and Applications, 2012, 3, 326-331 /10.4236/msa.2012.35048 Published Online May 2012 (http://www.SciRP.org/journal/msa) Effect of Sintering Temperature on Structural and Magnetic Properties of Ni Zn Fe O Ferrites 0.55 0.45 2 4 1* 1 2 2 1 Robiul Islam , Md Obaidur Rahman , M. Abdul Hakim , Dilip Kumar Saha , Saiduzzaman , Saroaut Noor3, Md Al-Mamun2 1The Department of Physics, Jahangirnagar University, Dhaka, Bangladesh; 2Materials Science Division, Atomic Energy Centre, Dhaka, Bangladesh; 3Department of Physics, Khulna University of Engineering Technology, Khulna, Bangladesh. * Email: robiulislam41@ Received December 23rd, 2011; revised February 17th, 2012; accepted March 18th, 2012 ABSTRACT The effect of frequency and sintering temperature on initial permeability of Ni Zn Fe O ferrites have been studied 0.55 0.45 2 4 by using an impedance analyzer. The samples were prepared by conventional double sintering ceramic technique using oxide nanoparticles of grain size 30 - 50 nm. Single phase spinal structure has been confirmed for the prepared samples by X-ray diffraction. As the sintering temperatures increase from 1160˚C to 1300˚C, the permeability gradually in- creases. The increase of permeability is ascribed to the increase of density and grain size. Grain size is expected to grow with the increase of sintering temperature. Ferrites with large average grain size posses higher initial permeability. The Curie temperatures determined from temperature dependence