原创力文档effect of ultrasonic irradiation on preparation and properties of ionogels超声辐照对ionogels的制备和性质的影响.pdfVIP
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effect of ultrasonic irradiation on preparation and properties of ionogels超声辐照对ionogels的制备和性质的影响
Hindawi Publishing Corporation
Journal of Nanomaterials
Volume 2012, Article ID 570719, 6 pages
doi:10.1155/2012/570719
Research Article
Effect of Ultrasonic Irradiation on Preparation and
Properties of Ionogels
Yogendra Lal Verma, Manish Pratap Singh, and Rajendra Kumar Singh
Ionic Liquid and Solid State Ionics Laboratory, Department of Physics, Banaras Hindu University, Varanasi 221005, India
Correspondence should be addressed to Rajendra Kumar Singh, rksingh 17@rediff
Received 22 August 2011; Revised 25 October 2011; Accepted 29 October 2011
Academic Editor: Jaetae Seo
Copyright © 2012 Yogendra Lal Verma et al. This is an open access article distributed under the Creative Commons Attribution
License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly
cited.
Silica-gel matrices containing ionic liquid (IL) 1-butyl-3-methylimidazolium hexafluorophosphate viz. ionogels have been
synthesized using one-pot nonhydrolytic sol-gel method and taking tetraethyl orthosilicate (TEOS) as starting precursor. Effect
of ultrasonic irradiation on pore parameters of ionogels and vibrational properties of the IL upon confinement in the porous
matrix has been investigated. The synthesized gels have been characterized by BET, DSC, TGA, and FTIR. BET analysis shows
some changes in the pore parameters due to ultrasonic irradiation. DSC results indicate shift in glass transition temperature upon
confinement of the IL. The FTIR spectra show changes in vibrational bands on confinement, particularly, the bands related to
the imidazolium ring; aliphatic chain and anion PF6 − of the IL are found to shift upon confinement in porous silica matrix
obtained due to ultrasonic irradiation. Ultrasonic irradiation has been fou
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