effect of zn substitution on the magnetic properties of cobalt ferrite nano particles prepared via sol-gel route影响锌替代钴铁氧体的磁性纳米粒子通过溶胶-凝胶法路线准备.pdfVIP

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effect of zn substitution on the magnetic properties of cobalt ferrite nano particles prepared via sol-gel route影响锌替代钴铁氧体的磁性纳米粒子通过溶胶-凝胶法路线准备.pdf

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effect of zn substitution on the magnetic properties of cobalt ferrite nano particles prepared via sol-gel route影响锌替代钴铁氧体的磁性纳米粒子通过溶胶-凝胶法路线准备

J. Electromagnetic Analysis Applications, 2010, 2, 376-381 doi:10.4236/jemaa.2010.26049 Published Online June 2010 (http://www.SciRP.org/journal/jemaa) Effect of Zn Substitution on the Magnetic Properties of Cobalt Ferrite Nano Particles Prepared Via Sol-Gel Route 1 1 2 3 Sonal Singhal *, Tsering Namgyal , Sandeep Bansal , Kailash Chandra 1Department of Chemistry, Panjab University, Chandigarh, India; 2Department of Metallurgical and Materials Engineering, Indian Institute of Technology-Roorkee, Roorkee, India; 3Institute Instrumentation Centre, Indian Institute of Technology-Roorkee, Roorkee, India. Email: sonal1174@ Received February 22nd, 2010; revised April 15th, 2010; accepted April 22nd, 2010. ABSTRACT Zinc substituted cobalt ferrite nanoparticles (Co Zn Fe O , with x = 0.0, 0.2, 0.4, 0.8 and 1.0) were prepared via sol-gel x 1-x 2 4 route and the effect of zinc concentration on saturation magnetization and lattice parameter were investigated. The parti- cle sizes of the as obtained samples were found to be ~10 nm which increases upto ~92 nm on annealing at 1000oC. The -1 -1 frequency bands near 564-588 cm and 425-442 cm are assigned to the tetrahedral and octahedral clusters which con- firm the presence of M-O stretching band in ferrites. The unit cell parameter ‘a’ increases linearly with increasing con- centration of zinc due to larger ionic radii of Zn2+ ion . It was found that this substitution allows tunable changes in the magnetic properties of cobalt ferrite. Interestingly, saturation magnetization first increases upto x = 0.4 and then de- creases for higher Zn substitution, thus tunable changes in magnetic properties of cobalt ferrite ar