超声波辅助提取黄秋葵籽油及其脂肪酸组成分析 ultrasonic - assisted extraction of abelmoschus esculentus seed oil and its fatty acid composition.pdfVIP

14 CHIＮA OILS AＮD FATS 2014 Vol．39 Ｎo．8 油脂加工 超声波辅助提取黄秋葵籽油及其脂肪酸组成分析 唐 萍，鲜欣言，胡怀容，张友华，李明元 (西华大学生物工程学院，成都610039) 摘要:采用超声波辅助提取黄秋葵籽油并采用GC-MS对其脂肪酸组成进行分析。 通过单因素试 验考察提取溶剂、原料粒度、料液比、提取温度、提取时间、超声功率对黄秋葵籽油得率的影响。 在 单因素试验基础上采用正交试验优化得到最佳提取工艺条件为:正己烷为提取溶剂，原料粒度40~ 60 目，料液比1：9，提取温度50℃，提取时间75 min，超声功率80 W。 在最佳条件下，黄秋葵籽油得 率为26．26%。 从黄秋葵籽油中鉴定出11种脂肪酸，主要为不饱和脂肪酸，含量最高的为亚油酸， 占34．06%。 关键词:黄秋葵籽油;超声波提取;脂肪酸组成 中图分类号:TS224;TQ646 文献标志码:A 文章编号:1003-7969(2014)08-0014 -04 Uｌｔraｓoniｃ－aｓｓiｓｔｅｄ ｅxｔraｃｔion oｆAbelmoschus esculentus ｓｅｅｄ oiｌ anｄ iｔｓ ｆaｔｔy aｃiｄ ｃoｍｐoｓiｔion TAＮG Ping,XIAＮ Xinyan,HU Huairong,ZHAＮG Youhua,LI Mingyuan (School of Bioengineering,Xihua University,Chengdu610039,China) Aｂｓｔraｃｔ：Theultrasonic-assisted extraction ofAbelmoschus esculentus seed oilwasstudied andthefatty acid composition of Abelmoschus esculentus seed oil was analyｚed by GC-MS． The effects of extraction solvent,material granularity,ratio of material to liquid,extraction temperature,extraction time and ul- trasonic power on the yield of Abelmoschus esculentus seed oil were studied by single factor experiment． Then the ultrasonic-assisted extraction conditions were optimiｚed by orthogonal experiment as follows： with n-hexane as extraction solvent,material granularity 40 -60 meshes,ratio of material to liquid 1：9,extraction temperature 50℃,extraction time 75 min,ultrasonic power 80 W． Under the optimal conditions,theyieldofAbelmoschus esculentus seedoilwas26．26%,andelevenkindsoffatty acidswere identified fromAbelmoschus esculentus seedoil,amongwhichthecontent of linoleicacidwasthehighest, reaching34．06%． Kｅy ｗorｄｓ：Abelmoschus esculentus seed oil;ultrasonic-assisted extraction;fatty acid composition