利用高铝粉煤灰制备莫来石微晶玻璃的试验研究-欢迎访问矿物岩石.PDFVIP

# # Bu lletin of M ineralogy , Pet rology and Geoch emis t ry V ol. 25 No . 4, Oct . 2006 刘 浩, 马鸿文, 彭 辉, 俞子俭, 苏双青 , 1000 83 以高铝粉煤灰为主要原料, 采用粉末烧结法制 出莫来石微晶玻璃X 射线衍射分析显示, 经1350 ~ 1550 e 热处理 后, 制得的微晶玻璃的主晶相均为莫来石扫描电镜分析表明, 较高的温度下热处理有利于晶体的生长微晶玻璃的理化性 能如吸水率气孔率体积密度抗折强度和化学稳定性, 随热处理温度的不同而发生相应的变化1500 e 热处理 2 h 制得的 微晶玻璃具有优良的理化性能, 在工程和结构领域具有潜在的应用前景 莫来石微晶玻璃; 高铝粉煤灰; 粉末烧结 P 579 A 1007- 2802 ( 200 6) 04- 0 35 3- 04 Preparation of Mullite Glass-ceramicsfrom High AluminaFlyAsh: An Experimental Study LIU H ao, M A H o ng- w en, PEN G H u i, Y U Z-i jian, SU Shuang- qing N ational L abor atory of M iner al M ater ials , China Univ ersity of Geosc iences , Beij ing 1000 83, China Abstract: T he mullit e glas s- ceram ics w as prepared w it h high alum ina f ly ash as principal raw m aterials by p ow der sin tering m et hod. X- ray dif fract ion analy sis ( XRD) result s show that th e crys tal phase of the glass-ceram ics p re- pared b y heating at temp erat ure ran ging f rom 1350 e to 1550 e w as only mu llite . Scannin g elect ron m icroscopy ( SEM ) ob servat ion indicat ed t hat t he heating t reat m ent at h igher temperat ure is favorable for t he cry stal grow t h. T he phy sicochem ical propert ies of glass- ceram ics, such as w at er ab sorpt ion, porosit y , apparent densit y , bending strength and chem ical stability w ere varied w ith th e variat ion of h eat ing treatm ent t emperat ures. T he glass- ceram- ics prep ared by heating treatm ent at 1500 e for 2 hour s show t hat it has good p ropert ies and w ill h ave att ract ive po- t ent ials for engin