正丙醇提取茶皂素工艺 Optimization of Extraction Process for Tea Saponin from Camellia oleifera Seed Meal with n-Propanol.pdfVIP
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正丙醇提取茶皂素工艺 Optimization of Extraction Process for Tea Saponin from Camellia oleifera Seed Meal with n-Propanol
582013,V01.34,No.02 良晶科学 ※工艺技术
正丙醇提取茶皂素工艺
于辉,陈海光,吴波,任文彬
(伸恺农业工程学院轻工食品学院,广东广州 510225)
摘要:采用正丙醇浸提提取油茶籽粕中的茶皂素。考察原料颗粒的目数、浸提液正丙醇溶液的体积分数、料液比、
浸提时间、浸提温度以及浸提液pH值对提取效果的影响,并用正交试验获得最佳工艺。以茶皂素得率为优化对象时,
件下,茶皂素纯度72.06%、得率15.31%。上述工艺所得茶皂素产品的得率及纯度均优于常规乙醇浸提法。
关键词:茶皂素;正丙醇;提取.
ofExtractionfor Camellia
ProcessTea from Meal
oleifer口Seed
Optimization Saponin with,z—Propanol
YU
Hui,CHEN Bo,RENWen—bin
Hai—guang,WU
of andFood of and 5
(CoHegeLightIndustry Science,ZhongkaiUniversityAgricultureEngineering,Guangzhou10225,China)
wasusedtoexlraettea fromoil that
Abstract:n-Propanol sapom tea(CamelliaoleiferaAbel.)seed
meal.Operatingparameters
influenceextraction suchaslawmaterial concentlation,solid-to-solvent
efficiency particlesize,n-propanol ratio,time,temperature
andsolventwere one-factor-at-a-timemethodand an
investigatedby optimized design.The
pH usingorthogonalarray optimum
formaximum
extractionconditions oftea werefoundtobe60 3hforlaWmaterial
yield saponin mesh,80%,1:12(g/mL),80℃and
and the and oftea obtainedunder
coneentrafion,temperature saponin
particlesize,n-propanol time,respectively,andyieldpurity
theseconditionswere20.13%and extractionconditionsformaxlnl
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