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英文文献翻译硼作显色剂在分光光度计法中的应用一项有关氨甲苯酸与硼酸为定作用的新颖的褪色分光光度计法
英文文献
Journal of the Chinese Chemical Society,2007,54,983-990 983
Application of Boron as the Chromogenic Agent in Spectrophotometry
A Novel Fading Spectrophotometric Method for the Determination of Aminomethylbenzoic Acid with Boric Acid
Quan-Min Li* ( ) and Tian-Tian Zhang ( )
College of Chemistry and Environmental Science, Henan Normal University; Henan Key Laboratory for Environmental Pollution Control, Xinxiang, Henan 453007, P. R. China
It is the first time that boron has been used as a chromogenic agent to determine aminomethylbenzoic acid (PAMBA) by the fading spectrophotometric method in this paper. The study indicates that at pH 10.00theabsorbance of PAMBA decreases when boric acid(BA) is added to the solution. A simple ,rapid, sensitive and reliable novel method based on the product of PAMBA and BA is obtained. The stoichiometric ratio of the product is 1:2. Beers law is obeyed in the range of PAMBA concentrations of 0.13~38.40μg/mL at a wavelength of 242nm(242 is 8.1×104L/mol/cm) The equation of linear regression is A=—0.06635—0.02914C (×10-5 M), with a linear correlation coefficient of 0.9974. The detection limit is 0.12μg/mL and RSD 0.11%.The method is successfully applied to the determination of PAMBA in pharmaceutical samples, and average recoveries from pharmaceutical samples and urine samples were between 98.4~02.5%. The other components in these samples do not interfere with the determination by the proposed method.
Keywords: Boron; Aminomethylbenzoic acid; Chromogenic agent; Fading spectrophotometric method.
INTRODUCTION
Boron is an electron lacking element , and has a strong ability of accepting electrons. It is easy for boron to form a polymetric molecule or a steady complex with an electron donor. The complex characteristic of boron is of important meaning for the study of its biochemical effects and nutrition physiology to plants in life science.
Up to the present, a number of specific reagents used to determine boron by spetrophotometric me
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