工业废盐酸浸出低品位菱锰矿制取四水氯化锰的扩大试验研究.pdf

贵州大学硕士论文 pollution of natural environment, the source comprehensive utilization can be implemented. The research contents of this paper include enlarged experiment research and circulation research and purification research. The influences of the index of excessive acid, ratio of liquid and solid, temperature and time were investigated by single factor experiment and orthogonal designed experiments on the manganese leaching rate in the leaching during the enlarged experiment research, then finally ascertain the best leaching process factors. The circulation research confirms the reasonable circulation process by investigating circulation method and ratio of return solution, which can reduce resource consumption and improve production efficiency.The most reasonable purification method can be acquired by reviewing purification of leaching process and leaching solution during the purification research. Under the Laboratory basic research before, the abundance of low-grade rhodochrosite in Guizhou province can be made full used , combined with industrial waste hydrochloric which is produced from the production of sponge titanium. H O 2 2 can be used as oxidant, enlarged experiment research is studied to gain four water chloride manganese. The best leaching process factors of enlarged experiment research acquired are as follows after single factor experiment and orthogonal designed experiments which contains four factors and three levels: temperature is 80 ℃, time is 50 min, ratio of liquid and solid is 4:1 and leaching process Ph is from 2.5 to 3.0.Under the conditions, the leaching efficiency