压榨法提取生姜挥发油的工艺研究.docVIP

压榨法提取生姜挥发油的工艺研究 CJCM中华实用中西医杂志2006年VOL.(19)NO.21 压榨法提取生-g挥发油的工艺研究 StudVonextractiontechnology ofvolatileOi1jjrOmRhizomaZingiberiSRecens 丈红梅王跃飞王永山郭立玮 (南京中医药大学,江苏,南京,210029) WENHongmei,WANGYuefei,WANGYongshang,GOULiwei (NanjingUniversityofTCM,Nanjing210029,China) 中图分类号:R283文献标识码:A文章编号:1607—2286(2o06)21—2605-04 【摘要】目的压榨法提取生姜挥发油的工艺研究.方法采用水蒸汽蒸馏法,压榨法两种提取方法,对同一批次的生姜 样品进行提取.采用高效液相色谱法和气相色谱法对提取液进行成分分析,考察压榨法提取生姜挥发油的可行性.采用正交试验 优化了生姜汁中生姜挥发油的B一环糊精包合工艺.结果压榨法提取的生姜汁中所含挥发油保留了传统水蒸汽蒸馏法的挥发油成 分,最佳包合工艺条件为一环糊精与生姜汁的比例为4:100,温度为50(2,包合时间为1h.结论压榨法具有操作方便,能耗低, 污染少的特点,适用于生姜挥发油的提取,采用B一环糊精包合技术能更有效地保留挥发性成分. 【关键词l生姜;挥发油;压榨法;提取工艺 [AbstractlObjective:TostudyonextractiontedmologyofvolatileoilfromRhizomaZingiberisReeensbysquashingextraction method.Methods:VolatileoilofRhizomaZingiberisReeensofthesanlebatchWaSextractedusingsteamdistillation,squashingextraction. ThechemicalconstituentsofvolatileoilextractedbythosemethodswereanalyzedbyHPLCandGC.ItWaSdemonstratedthatsquashing extractionWaSfeaSibleforextractionofvolatileoilfromRhizomaZingiberisRecens.Optimumparametersofinclusionofvolatileoilwere selectedbyorthogonaltest.Results:Volatileoilextractedbysquashingex~actionwasasgoodasextractedbysteamdistillation.Volatile oilfromRhizomaZingiberisReeenspreparedbysquaShingextractionwereincludedwithI~-cyclodextrin.Theoptimumparametersof inclusionWaSasfollow:theratioof-cyclodextrinandgingerjuiceWaS4:100,thetemperatureofinclusion50C,thetimeofinclusionlh. Conclusion:Squashingextractionisnewextractiontechnologyforextractingvolatileoilfromginger,whichischaracterizedbysimple operation,lowenergy-consumingandfreeorganicpollution.TheoptimumprocessofinclusionisfeaSible,whichcouldeffectively m~minthechemicalconstituentsofvolatileoilofRhizomaZingiberisRecens. [Keywords]RhizomaZingiberisRecens,valotileoil,squashingextraction,extractiontechnology 生姜为姜科植物姜ZingiberofficinaleRose.新鲜根茎. 具有解表散寒,温中止呕,化痰止咳的功效.用于风寒感冒, 胃寒呕吐,寒痰咳嗽.生姜主要含挥发性成分如姜烯,姜醇, 桉叶油素,柠檬烯,芳樟醇等数十种,还含有辛辣成分如姜辣 醇,姜辣二醇,姜辣烯酮等,其中部分生姜辣味成分的挥发性 较低.生姜挥发油的提取工艺以水蒸汽蒸馏法为主,也有采 用超临界流体萃取制备生姜