苯与氯苯分离过程板式精馏塔设计.docxVIP

题目苯-氯苯分离过程板式精憎塔设计 指导教师 辅导教师 学生姓名 学生学号 院（部） 专业 班 年—月—_日 苯-氯苯分离过程板式精憎塔设计 摘要 本设计为设计一个精馆塔来进行苯■氯苯混合物的分离，采用连续操作 方式的筛板精馆塔。在常压下，采用泡点进料，连续精憾方式，将原料通过 预热器加热至泡点后送入精馆塔内原料液连续加入精馆塔中，以一定得回流 比由连续精馆塔的塔顶采出含量合格的苯，由塔底采岀氯苯。并连续收集产 物和排出残液氯苯纯度不低于99.8%，塔顶产品苯纯度不低于98% （质量分 数）。近年来，我国氯苯系列产品产能扩增迅猛，主要品种产能和产量己居 世界第一，成为全球氯苯系列产品主耍的生产国和供应国，生产能力占全球 总生产能力的50%以上。氯苯系列产品的快速发展，对我国医药、农药、染 料、橡胶助剂、合成新材料等行业的发展也起着举足轻重的作用。目前国外 对、邻硝基氯苯的发展呈现衰减趋势，主要依靠进口国内的对、邻硝基氯苯 生产下游精细化学品，如染/颜料、医药、农药等。 关键）司：苯■氯苯；分离过程；板式精憾塔; The Design Process of Benzene And Chlorobenzene Separation Plate Distillation Tower ABSTRACT Separation of the design for a distillation tower of benzene and chlorobenzene mixtures, continuous operation of sieve plate distillation method. Under normal pressure, the bubble point feed, continuous distillation, the raw material through the preheater after heated to soak into the distillation tower material liquid continuous addition of rectification tower, reflux ratio content to have qualified benzene produced by continuous distillation tower from the tower bottom, chlorobenzene production. And continuously collecting product and discharge the residual liquid chlorobenzene purity of not less than 99.8%, the product of benzene purity of not less than 98% (mass fraction). In recent years, the capacity of chlorobenzene series products in China was rapid, the main varieties of production capacity and output has ranked first in the world, become the world of chlorobenzenes major producers and suppliers, production capacity accounted for the total global production capacity of more than 50%. The rapid development of chlorobenzene series products, development of Chinese medicine, pesticides, dyes, rubber additives, synthesis of new materials and other industries also play a decisive role. At present, development of nitrochlorobcnzcnc abroad demonstrates the attenuation trend, mainly rely on imports, domestic on o nitrochlorobcnzcnc production downstream fine chemicals, such as medicine, pesticide, dye/Pigment etc