英文版论文资料：Accuracy verification and practice of simultaneous thermal analyzer.pdfVIP

ISSN1002-4956实验技术与管理第42卷第11期2025年11月

CN11-2034/TExperimentalTechnologyandManagementVol.42No.11Nov.2025

DOI:10.16791/j.cnki.sjg.2025.11.015

Accuracyverificationandpracticeofsimultaneousthermalanalyzer

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LIHaixia,YANGXiuhong(),TIANLiyan,LUOMinting,GUOYanwen

(1.InstituteofProcessEngineering,ChineseAcademyofScience,Beijing100190,China;

2.SchoolofEnvironmentandSpatialInformatics,ChinaUniversityofMiningandTechnology,Xuzhou221116,China)

Abstract:Theaccuracyofthermalanalysismeasurementsiscriticaltoanalyzematerialpropertiescorrectly,makingtheimprovementof

measurementprecisionandproperuncertaintyanalysisoftestresultsabsolutelyessential.Asaprimarythermalanalysisinstrument,the

simultaneousthermalanalyzer(STA)hasuniqueadvantages,whichcombinesthefunctionalitiesofthermogravimetric(TG)analyzersand

differentialscanningcalorimeters(DSC).However,theabsenceofstandardqualitycontrolprocedureshasresultedinpoormeasurement

reproducibility,lowaccuracy,andinadequatetraceabilityofanalyticalresults.Thisstudyutilizedamulti-pointtemperaturecalibration

methodbasedonnationalcertifiedreferencematerialstoreduceinstrumenttemperatureindicationerrors.Onthisbasis,weinnovatively

establishedacomprehensivequalitycontrolsystemencompassinglaboratoryenvironmentalcontrol,standardmethodselection,instrument

performanceverification,referencematerialtraceabil