膏体尾矿屈服应力检测及其优化.docVIP

第 44 卷第 8 期 2013 年 8 月  中南大学学报(自然科学版) Journal of Central South University (Science and Technology)  Vol.44 No.8 Aug. 2013  膏体尾矿屈服应力检测及其优化 吴爱祥，焦华喆，王洪江，李辉，仪海豹，刘晓辉，刘斯忠 (北京科技大学土木与环境工程学院，金属矿山高效开采与安全教育部重点实验室，北京，100083) 摘要：屈服应力是高浓度非牛顿膏体的关键流变参数，是管道输送系统设计的基础，但目前该参数的实验获取不 准确。针对桨式流变仪操作方法不同带来的屈服应力检测结果差距较大的问题，引入塌落度屈服应力理论对上述 差异进行检验和校正，从而得到较为准确的浆体屈服应力和仪器操作方法。首先用控制剪切应力法(CSS)和控制 剪切速率法(CSR)操作桨式流变仪检测屈服应力，然后利用塌落度流变理论所得屈服应力对桨式屈服应力进行对 比分析。研究结果表明：塌落度法所得结果为浆体的动态屈服应力，CSS 法流变曲线回归所得的宾汉姆屈服应力 为静态屈服应力，并推荐恒定剪切速率的 CSR 法所得动态屈服应力能够反映物料性质，且剪切速率越低(＜0.05 s ?1 )，检测结果越准确。 关键词：膏体尾矿；屈服应力；桨式流变仪；塌落度流变理论；检测方法 中图分类号：O373；TD926；TQ177.6 文献标志码：A 文章编号：1672?7207(2013)08?3370?07  Yield stress measurements and optimization of Paste tailings WU Aixiang, JIAO Huazhe, WANG Hongjiang, LI Hui, YI Haibao, LIU Xiaohui, LIU Sizhong (State Key Laboratory of Ministry of Education of China for High-Efficient Mining and Safety of Metal Mines, School of Civil and Environmental Engineering, University of Science and Technology Beijing, Beijing 100083, China) Abstract: Yield stress is the key parameter of high concentration non-Newton Paste, and the fundament for pipeline system design. But presently the value obtained from experimental test is not precise. For the disunity between the values from different test methods, the slump rheology theory was brought in for verifying and revising the disunity, furthermore, more exact yield stress value was obtained and the operation method of rheometer was commended. Firstly, the samples’ yield stress was tested with vane rheometer, which was operated by Controlled shear stress (CSS) model and Controlled shear rate (CSR) model. Secondly, the values were compared with slump test results from the slump rheology theory. At last, the more exact yield stress value and more rational operation could be obtain. The results show that the value test by slump is the dynamic yield stress of sample, and the Bingham yield stress extrapolated from the rheol