Mechano-chemical method assisted extraction of total flavonoids of Technology Ciwujia.docVIP

 PAGE \* MERGEFORMAT 11 Mechano-chemical method assisted extraction of total flavonoids of Technology Ciwujia Author: Liu Ying Li-Ji Jin Xu Yongping Wang Xiaoyan Song Chunna [Abstract] Objective To study the mechanical-chemical method assisted extraction of total flavonoids Ciwujia the optimum. Method to study the extraction rate of total flavonoids of indicators, through a single factor and orthogonal experimental study mechanical-chemical method assisted extraction of total flavonoids Ciwujia the main factors to determine the optimum process conditions; using spectrophotometric determination of total flavonoids. Results optimum conditions: Na2CO3/Na2B4O7 additive amount of 4% (W / W), materials, particle size D95 ≤ 37 μ m, ethanol concentration 20% (V / V), solid-liquid ratio of 1:60 (g: ml). The process conditions, the extraction yield of flavonoids increased heat reflux 13.2%. Conclusion mechano-chemical method assisted extraction with high extraction rate, the time is short, no heat, ethanol, etc. with less features, the extraction of Acanthopanax an effective method for total flavonoids. [Keywords:] mechanical-chemical method assisted extraction of total flavonoids orthogonal Ciwujia Abstract: ObjectiveTo optimize the mechanochemical assisted extraction on the total flavonoids from Eleutherococcus senticosus. Methods The optimum extraction parameters were investigated by one-factor experiment and orthogonal design. The content of total flavonoids was determined by spectrophotometry. Results The optimum parameters were as follows: Na2CO3/Na2B4O7 content 4% (W / W), particle size D95 ≤ 37 μ m, 20% (V / V) ethanol, solid / liquid ratio 1:60 (g: ml). Under these parameters, the total flavonoids yield increased by 13.2% compared with heat-reflux extraction. ConclusionThe mechanochemical assisted extraction can improve the total flavonoids yield, shorten the extraction time, reduce the ethanol consumption, and need no heat. It is an effective method for t