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HPLC法测定当归芍药散中芍药苷的含量.pdf
HPLC 娉曟祴瀹氬綋褰掕妽鑽暎涓妽鑽嫹鐨勫惈閲徫
锛 2锛? 锛? 锛? #
鍛 鐝 锛岀帇 鐧 锛屽紶 榛 锛屽紶 閿 锛屾潕鑼傛槦 锛屽紶姹濆 锛岃淳姝e钩 锛?.鍏板窞鍐涘尯鍏板窞鎬诲尰闄㈠叏鍐涢珮鍘熺幆澧冩崯
浼ら槻娌婚噸鐐瑰疄楠屽/ 鍥藉涓尰鑽鐞嗗眬涓村簥涓嵂瀛﹂噸鐐瑰绉戯紝鍏板窞 730050锛?.鐢樿們涓尰瀛﹂櫌鑽闄紝鍏板窞
730000锛?.瑗垮畨澶у叴鍖婚櫌鑽墏绉戯紝瑗垮畨 710016锛
涓浘鍒嗙被鍙 R917 鏂囩尞鏍囧織鐮 A 鏂囩珷缂栧彿?016锛?0425503
DOI 10.6039/j.issn.2016.30.25
鎽 瑕 鐩殑锛氬缓绔嬫祴瀹氬綋褰掕妽鑽暎涓妽鑽嫹鍚噺鐨勬柟娉曪紝浠ユ湡涓烘帶鍒惰鍒跺墏鐨勮川閲忔彁渚涘弬鑰冦€傛柟娉曪細閲囩敤楂樻晥娑茬浉鑹茶氨娉曘€傝壊
璋辨煴涓篠ymmetry C18锛屾祦鍔ㄧ浉涓轰箼鑵堟按锛堝惈0.1锛呯7閰革級锛?4鈭?6锛孷/ V锛夛紝娴侀€熶负1.0ml/min 锛屾娴嬫尝闀夸负230nm 锛屾煴娓╀负20 鈩冿紝杩涙牱閲
涓?0渭l銆傜粨鏋滐細鑺嶈嵂鑻锋娴嬭川閲忔祿搴︾嚎鎬ц寖鍥翠负10锝?0渭g/ml 锛坮 锛?.9993锛夛紱绮惧瘑搴︺€佺ǔ瀹氭€с€侀噸澶嶆€ц瘯楠岀殑RSD 锛?锛咃紱鍔犳牱鍥炴敹
鐜囦负98.3锛咃綖104.9锛咃紙RSD 锛?.0锛咃紝n 锛?锛夈€傜粨璁猴細璇ユ柟娉曠畝渚裤€佸噯纭€佷笓灞炴€у己锛屽彲鐢ㄤ簬娴嬪畾褰撳綊鑺嶈嵂鏁d腑鑺嶈嵂鑻风殑鍚噺銆
鍏抽敭璇 褰撳綊鑺嶈嵂鏁o紱鑺嶈嵂鑻凤紱楂樻晥娑茬浉鑹茶氨娉曪紱鍚噺娴嬪畾
Content Determination of Peoniflorin in Danggui Shaoyao Powder by HPLC
ZHOU Jun 锛學ANG Deng2锛?锛孼HANG Li 锛孼HANG Jin 锛?锛孡I Maoxing 锛孼HANG Ruxue 锛?锛孞IA Zhengping 锛?.Key
Laboratory of the Prevention and Cure for the Plateau Environment Damage 锛孡anzhou General Hospital of Lan-
zhou Military Region/Key Disciplines of Clinical Chinese Materia Medica 锛孲tate Administration of TCM 锛孡an-
zhou 730050锛孋hina 锛?.College of Pharmacy 锛孏anSu University of Chinese Medicine 锛孡anzhou 730000锛孋hina 锛?.
Dept. of Pharmacy 锛孹i 鈥檃n Daxing Hospital 锛孹i 鈥檃n 710016锛孋hina 锛
ABSTRACT OBJECTIVE 锛歍o establish a method for the content determination of peoniflorin in Danggui shaoyao powder 锛宎nd
provide a reference for controlling the quality of the preparation. METHODS 锛欻PLC was performed on the column of Symmetry
C18 with mobile phase of acetonitrile water 锛坈ontaining 0.1锛卲hosphoric acid 锛夛紙14鈭?6锛孷/ V锛塧t a flow rate of 1.0 ml/min 锛宒etection
wavelength was 230nm 锛宑olumn temperature was 20 鈩冿紝and injection volume was 20 渭l. RESULTS 锛歍he linear range of peoniflo
rin was 1080 渭g/ml 锛坮 锛?.999 3锛夛紱RSDs of precision 锛宻ta
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