原创力文档effect of sample matrix on radial and axial profiles of ion abundance in inductively coupled plasma mass spectrometry样本矩阵的影响在径向和轴向的离子丰度在电感耦合等离子体质谱法.pdfVIP
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effect of sample matrix on radial and axial profiles of ion abundance in inductively coupled plasma mass spectrometry样本矩阵的影响在径向和轴向的离子丰度在电感耦合等离子体质谱法
American Journal of Analytical Chemistry , 2011, 2, 739-751
doi:10.4236/ajac.2011.27085 Published Online November 20 11 (http://www.SciRP.org/journal/ajac)
Effect of Sample Matrix on Radial and Axial Profiles of
Ion Abundance in Inductively Coupled Plasma
Mass Spectrometry
1* 2 1
Clarisse Mariet , Francine Carrot , Mélanie Moskura
1
Laboratoire Interdisciplinaire sur l ’Organisation Nanométrique et Supramoléculaire (LIONS),
CEA Saclay Gif-sur Yvette, France
2 UMR 3299, CEA Saclay Gif-sur Yvette, France
*
E-mail: clarisse.mariet@cea.fr
Received April 30, 2011; revised June 26, 2011; accepted July 8, 2011
Abstract
In inductively coupled plasma mass spectrometry (ICP-MS) analysis, only a few options are available to deal
with non-spectroscopic interferences. Considering that diluting the sample is impractical for traces analysis,
other alternatives must be employed. Traditionally, the method of standard additions is used to correct the
matrix effect but it is a time consuming method. Others methods involves separation techniques. Another
way to overcome matrix interferences is to understand the mechanism involved and adjust plasma viewing
conditions to reduce or eliminate the effect. In this study, the effect of various concomitant elements in
ICP-MS was assessed by measuring the distribution of selected singly charged analyte ions (Al, V, Cr, Mn,
Ni, Co, Cu, Zn, As, In, Ba, La, Ce, Pb), doubly charged ions (La, Ce, Ba and Pb) and oxides ions (BaO) in
the presence of conco
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