non-destructive evaluation of historical paper based on ph estimation from voc emissions无损评价的历史基础上的ph值估计从voc的排放.pdfVIP

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non-destructive evaluation of historical paper based on ph estimation from voc emissions无损评价的历史基础上的ph值估计从voc的排放.pdf

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Sensors 2007, 7, 3136-3145 sensors ISSN 1424-8220 © 2007 by MDPI /sensors Full Research Paper Non-Destructive Evaluation of Historical Paper Based on pH Estimation from VOC Emissions 1,* 2 3 4 2 Matija Strlič , Irena Kralj Cigić , Jana Kolar , Gerrit de Bruin and Boris Pihlar 1 University College London, Centre for Sustainable Heritage, The Bartlett School of Graduate Studies (Torrington Place site), Gower Street, London WCIE 6BT, UK, E-mail: m.strlic@ucl.ac.uk 2 University of Ljubljana, Faculty of Chemistry and Chemical Technology, Ljubljana, Slovenia E-mail:irena.kralj-cigic@fkkt.uni-lj.si; boris.pihlar@fkkt.uni-lj.si 3 National and University Library, Ljubljana, Slovenia, E-mail: jana.kolar@fkkt.uni-lj.si 4 Nationaal Archief, The Hague, The Netherlands, E-mail: gerrit.de.bruin@nationaalarchief.nl * Author to whom correspondence should be addressed. Received: 12 November 2007 / Accepted: 4 December 2007 / Published: 5 December 2007 Abstract: Volatile organic compounds (VOCs) emitted from materials during degradation can be a valuable source of information. In this work, the emissions of furfural and acetic acid from cellulose were studied using solid-phase micro-extraction (SPME) in combination with gas chromatography-mass spectrometry. Two sampling techniques were employed: static headspace sampling using SPME for 1 h at 40 oC after 18-h sample preparation