一系列新型单萘基不对称卟啉与新型β,β′-键联卟啉-二氢卟吩二聚体合成及表征-synthesis and characterization of a series of novel mono - naphthyl asymmetric porphyrins and novel β, β - linked porphyrins - chlorin dimer.docxVIP

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一系列新型单萘基不对称卟啉与新型β,β′-键联卟啉-二氢卟吩二聚体合成及表征-synthesis and characterization of a series of novel mono - naphthyl asymmetric porphyrins and novel β, β - linked porphyrins - chlorin dimer.docx

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一系列新型单萘基不对称卟啉与新型β,β′-键联卟啉-二氢卟吩二聚体合成及表征-synthesis and characterization of a series of novel mono - naphthyl asymmetric porphyrins and novel β, β - linked porphyrins - chlorin dimer

一系列新型单萘基不对称卟啉与新型β,β′-键联卟啉-二氢卟吩二聚体的合成及表征英文摘要byaone-potreactionwithpurechloroformassolvent.Thesecompoundshavebeencharacterizedby1HNMR,X-raycrystallographyandUV-visspectroscopy.Keywords:asymmetricporphyrin;β,β′-linked;bisporphyrin;synthesisWrittenby:GaohuiXuSurpervisedby:ChuanjiangHuIII目录第一章绪论···················································································11.1卟啉及其衍生物的简介······························································11.2卟啉类化合物的性质··································································21.2.1卟啉的物理性质·······························································21.2.2卟啉的化学性质································································31.3卟啉化合物的合成研究进展·························································4Rothemund法5Adler-Longo法5Lindsey法6Macdonald法71.3.5[3+1]合成法····································································81.3.6线型四吡咯合成法·····························································91.3.7微波激励法·····································································91.3.8其它方法·······································································101.3.9高分子型卟啉及其金属化合物的合成···································101.4本论文的研究意义及目的··························································101.5参考文献···············································································11第二章一系列单萘基不对称卟啉的合成及表征········································152.1引言·····················································································152.2不对称中位取代卟啉的研究意义与应用········································152.2.1在分析化学方面的应用······················································152.2.2在生物化学方面的应用······················································172.2.3在在分子识别方面的应用···················································172.2.4在光电化学方面的应用······················································182.3一系列单萘基不对称卟啉的合成·················································192.3.1试剂和仪器····································································192.3.2一系列单萘基不对称卟