锆基合金低能带电粒子辐照和原子氧侵蚀效应-材料工程专业论文.docxVIP

Abstra Abstract 万方数据 万方数据 Abstract The irradiation tests of 160keV proton and 120keV nitrogen ion as well as 5eV atomic oxygen (AO) exposure test were conducted on Zr702 and ZrTiAlV alloy, using low-energy charged particle irradiation equipment and atomic oxygen exposure equipment, respectively. The effects of low-energy charged particle irradiation and AO exposure on Zr-based alloy have been studied by means of metallographic microscope, graze small angle X-ray diffraction(GAXRD) and transmission electron microscope (TEM), X-ray photoelectron spectroscopy analyzer(XPS), nano-indentation machine, cryogenic temperature vacuum friction and wear machine and scanning electron microscope (SEM). Microstructure analysis results indicated that there was not new phase produced on the surface of Zr702 and ZrTiAlV alloy after proton irradiation and atomic oxygen exposure. But ZrN was found on the surface of Zr702, while AlN and TiN were found on the surface of ZrTiAlV alloy after nitrogen ion irradiation combined with atomic oxygen exposure. After the atomic oxygen exposure, denudation traces were present on the surface of Zr702 and ZrTiAlV alloy, and the roughness was found to reduce. The surface roughness of Zr702 and ZrTiAlV alloy increased obviously after charged particles irradiation combined with atomic oxygen exposure. Nano-indentation test results indicated that nano-hardness of Zr702 and ZrTiAlV alloy increased obviously after charged particle irradiation, and decreased obviously after atomic oxygen exposure. The combined effects of charged particle irradiation and AO exposure on nano-hardness come from the single effect, respectively. Due to generation of nitrides on surface induced by nitrogen ion irradiation, the nano-hardness of Zr702 and ZrTiAlV alloy was found to increase after nitrogen ion irradiation and atomic oxygen exposure. The friction test results indicated that the initial friction coefficient of Zr702 sample in air at room temperature of the charged pa