含钼多酸盐和银配合物的合成、晶体结构及性质研究-无机化学专业论文.docxVIP

万方数据 万方数据 A Thesis Submitted for the Degree of Master SYNTHESIS, CRYSTAL STRUCTURE AND PROPERTIES RESEARCH OF POLYOXOMETALATE CONTAINING MOLYBDENUM AND SILVER COMPLEXES Candidate ： Wei Wei Supervisor ： prof. Baibin Zhou Speciality ： Inorganic Chemistry Date of Defence ： June, 2012 Degree-Conferring-Institution ： Harbin Normal University 目 目 录 万方数据 万方数据 目 录 HYPERLINK \l _bookmark0 摘 要 ····························································································· I HYPERLINK \l _bookmark1 Abstract ······························································································ II HYPERLINK \l _bookmark2 第1 章 绪 论 ·······················································································1 HYPERLINK \l _bookmark3 1.1 同多钼酸盐的研究概况 ···································································1 HYPERLINK \l _bookmark4 1.2 小分子同多钼酸盐的研究 ································································ 3 HYPERLINK \l _bookmark5 1.3 多酸参与原位配体合成的研究 ··························································7 HYPERLINK \l _bookmark6 1.4 含钼 Anderson 化合物的研究概况 10 HYPERLINK \l _bookmark7 1.5 以银为中心原子配合物的研究概况 ·················································· 12 HYPERLINK \l _bookmark8 1.6 选题的依据及研究内容 ································································· 13 HYPERLINK \l _bookmark9 第 2 章 实验材料及测试方法 ································································· 15 HYPERLINK \l _bookmark10 2.1 实验材料及仪器设备 ···································································· 15 HYPERLINK \l _bookmark11 2.1.1 主要试剂 ·············································································· 15 HYPERLINK \l _bookmark12 2.1.2 主要仪器设备········································································· 15 HYPERLINK \l _bookmark13 2.2 测试方法··················································································· 16 HYPERLINK \l _bookmark14 2.2.1 红外光谱(IR)分析 16 HYPERLINK \l _bookmark15 2.2.2 差热-热重(TG-DTA)分析 16 HY