甲醛试纸的研制-药物分析专业论文.docxVIP

乙酸铵25％、乙酰丙酮2％；试纸的干燥方法为真空干燥法；滤纸的浸泡方法 乙酸铵25％、乙酰丙酮2％；试纸的干燥方法为真空干燥法；滤纸的浸泡方法 为直接浸泡法；合适的滤纸载体为中速定性滤纸以及浸泡合适次数为一次，使研 制的试纸达到最佳效果。同时确定了试纸的灵敏度为20 ppm，使用有效期暂定 为两个月，且最好置于阴凉处避光保存；因试纸实验室使用时其产生的颜色随浓 度梯度的变化改变不明显，自制试纸以定性为主。 最后，试纸的实用性检测：将自制甲醛试纸进行单盲实验和水发样品的实际 检测，结果：该试纸能将甲醛含量大于20 ppm的水发样品的蒸馏提取液检验出 来，且更易分辨含量大于50 ppm的蒸馏提取液；具有一定的应用性。 关键词：甲醛试纸 显色剂 条件优化 实用性检测 The The Test Paper for Formaldehyde Detecting Speciality：Pharmaceutical Analysis Author ：Li Jing-ping Supervisor：Professor Lu Tong-bu Senior Engineer Lu Hui-ning Abstract Formaldehyde，which is an achromatous and strong irritant gas，Can dissolve easily in water and ethanol and other organic solvents at roorfl temperature．It is widely used in industry．It’S also a high toxic subaance． The most common used method for detecting formaldehyde is eolorimetry,which is used in the hat,hal stand method for detecting formaldehyde in textile，food and air． In recent years，along with the progress of detecting technique，some more sensitive and quick detecting methods，such as GC，HPLC and GC—MS，are used for detecting formaldehyde，However,the above methods are not suitable for convenient and quick detecting．Therefore，a convenient and quick method for formaldehyde detecting，test paper,are investigated in this thesis． First of all，the different display reagents were investigated for formaldehyde detecting，and the modified acetyl acetone method showed the best result．The test paper produced under this condition showed the detecting limit of20 ppm． Secondly,the preparing conditions for test paper were optimized．The best condition is：anhydrous ethanol 10％，acetic acid ammonium 25％，acetyl acetone 2％， ．III． vacuum vacuum drying．and direct dipping Finally,the concen仃atmns of some food samples were determined by the above prepared test paper． Key Words：Test paper for detecting formaldehyde，display reagents， condition optimizing，application ．IV． 中山大学硕士学位论文 中山大学硕士学位论文 甲醛试纸的研制 第一章前言 甲醛，又名蚁醛：英文名称为：Formaldehyde或Methanal；化学式CH20， 分子质量30．03；常温下是一种无色、具有强烈刺激性的气体，熔点．92℃，