Flow injection on-line filtration-dilution atomic absorption spectrometry Ginkgo Flavonoids.docVIP

 PAGE \* MERGEFORMAT 10 Flow injection on-line filtration-dilution atomic absorption spectrometry Ginkgo Flavonoids Authors: Yang Li-Yan, with Jian-Bo, Jing-, LIU Chun-Ye [Abstract] Objective To establish a compound in Ginkgo biloba Ginkgo biloba method for determination of total flavonoids. Method in neutral medium, Ginkgo flavonoids with Cu2 association for the brown-yellow precipitate, after flow injection on-line filtering diluted to AAS determination of response to the remaining amount to indirect determination of Cu2 Ginkgo flavonoids content. Results ginkgo flavone concentration of 4.0 ~ 30 μ g / ml and reaction within the remaining amount of Cu2 showed good linear relationship, methods, the standard deviation of 1.1%, recovery 101% ~ 105%. Conclusion The method is simple and easy to implement automated, accurate, specific and strong, can be used as quality control of Ginkgo leaf. [Keywords:] Ginkgo flavonoids flow injection atomic absorption-line filtration Ginkgo Ginkgo biloba leaves, the main active substance is Ginkgo flavonoids (flavonoids), and ginkgo lactone compounds, studies have shown that ginkgo flavonoids can promote the metabolism of cardio-cerebral vascular system, as a plant-based drugs effective in promoting nerve endings and brain blood flow , for the treatment of cardiovascular diseases and Alzheimer’s disease and other ills with remarkable results [1], present its measurement methods are mainly high-performance liquid chromatography [2,3], UV spectrophotometry [4,5], fluorescence spectrophotometric method [6]. This article is in the neutral medium conditions, the use of Ginkgo flavonoids structure of the temporary phenol complexation with copper acetate to produce brown-yellow precipitate, using flow injection on-line filtration - atomic absorption spectrometry (FI-AAS) determination of the upper clear liquid remaining in the the amount of Cu2, which indirectly measured the content of flavonoids. The method is simple, fast, high