On Chinese Pharmacopoeia woody species identification reference SU Discussion Pill.docVIP

 PAGE \* MERGEFORMAT 4 On Chinese Pharmacopoeia woody species identification reference SU Discussion Pill [Abstract] lt;”China Pharmacopoeiagt;” -2005 edition Ⅰ Department, Su pills containing woody species parameter identification method to improve, the results show that: the improved method of chromatographic spots obtained clear and reproducible separation and negative non-interference. [Keywords:] Cf Su pill; lt;”China Pharmacopoeiagt;gt;; costas Su Wan closing argument contained in the lt;”China Pharmacopoeiagt;” -2005 edition of the Department Ⅰ, from Codonopsis, basil leaf, kudzu root, Peucedanum, woody smell of 11 herbs processed, mainly for physical weakness, feeling cold due to cold treatment [1]. during the inspection, we found differential (4) woody poor chromatographic separation of spots, so the agent was amended to put forward for peer discussion. An instrument and reagent Silica gel G thin layer plate (Qingdao Ocean Chemical Plant), balance (Mettler AE240); woody reference drug (in the inspection of the batch number :120921 -200,607), reagents were of analytical grade; Participation Su pill [Beijing Tong Ren Tang natural Drugs (Tangshan) Co., Ltd., batch number: 8085005,8085006,8085007]. 2 Methods and Results 2.1 The original method to take this product 7g, small study, add ethyl ether 25ml, dipping 4 h, always shaking, filtration, the filtrate evaporated to dryness, the residue add 1ml of ethanol allows the dissolved, the supernatant as the test solution. In another control woody herbs 0.5g, add ethyl ether 10ml, with the legal system medicine solution. According to thin layer chromatography (Appendix Ⅵ B) test, to learn the two solutions of the 2μl, respectively, points on the same silica gel G thin-layer board petroleum ether (60 ~ 90 ℃) - ethyl acetate (9:1) as the agent, started out, dried, sprayed with 1% vanillin sulfuric acid solution, heated at 105 ℃ to the spot color definition. for the test materials Chromatograph