氟硅唑在葡萄和土壤中残留的液相色谱分析方法.pdfVIP

2004, 6(2) : 8789 Chinese Journal of Pesticide Science 研究简报 * 陈　莉 ,　陈家梅, 　夏福利, 　戴荣彩, 　余苹中 ( , 100089) : , .010- 11 g, 0. 01 mg/ kg, 92. 6% 99.0% , 1.7% 1 . % : ; ; ; ; :T Q450. 6: A : 1008-7 0 ( 2004) 02-0087-0 Residue Analysis Method of Flusilazole in Grape and Soil by HPLC * CHEN Li , CHEN Jia-mei, XIA Fu-li, DAI Rong-cai, YU Ping-zhong (I ns tit ute of P lant P r otect ion and E nv ir onment P rotect ion , A cadem ic of B eij ing A g r icult ur al S cience ,B e ij ing 100089, China) Abstract: A method was developed to determine residue of flusilazole in grape and soil by HPLC. - 11 The low est detection limit of instrument for flusilazole w as . 010 g . The limit of quantita- tion w as 0. 01 mg/ kg. T he average recovery and coefficient of variation of this method w ere 92. 6% 99. 0% and 1. 7% 1 . % , respectively . HPLC system consisted of 15 cm4. 6 mm ( id ) Shim-pack VP ODS HPLC column equipped w ith a cm ODS guard column. Chro- matographic conditions as follow s: mobile phase, acetonitrile+ w ater (4555, V / V ) ; flow rate, 1 / ; , 45 ; , 195 . mL min column temperature detection w avelengths nm Key words: flusilazole; grape; soil; residue; HPLC (flusilazole) , , , 1 Sp haceloma amp el inum de Bary , Ventur ia p irina Aderh Sp haerotheca 1. 1 f olig enea ( Schlech) Poll. LC-10ATvp, , NP SPD-10A vp U V SIL-10ADvp [ 1] [ 2] - ; 1/ 10 , Class VP NP ,