【论文】苯氯化反应精馏过程自动控制系统设计与分析.pdfVIP

苯氯化反应精馏过程自动控制系统设计与分析　 冯康康,等 苯氯化反应精馏过程自动控制系统设计与分析 DesignandAnalysis of Automatic Control System for Benzene Chlorination Distillation Process 1 1,2 2 1 1 冯康康 　 薄翠梅 　 乔　 旭 　 李芳芳 　 张程浩 1 2 (南京工业大学自动化与电气工程学院 ,江苏 南京　 210009;南京工业大学化学与化工学院 ,江苏 南京　 210009) 摘　 要: 针对苯氯化连串汽液反应精馏过程的动态特性,在研究最佳反应精馏集成结构参数与操作参数的基础上,采用相对稳态增益矩 阵方法进行多回路控制系统被控变量与操作变量的合理配对,并分别设计了3种不同的控制方案(CS ~CS )。 对比分析了这3种控制1 3 方案在不同进料流率和成分扰动条件下的系统鲁棒性。 模拟结果表明,采用灵敏板温度调节进料比值控制与再沸器加热量控制塔釜质 量成分的配对结构模式(即CS 控制模式),闭环系统能获得较好的动态响应性能和鲁棒性。 3 关键词: 反应精馏　 过程自动控制　 多变量控制　 苯氯化　 灵敏度 中图分类号: TP273　 　 　 　 文献标志码: A Abstract: In accordance with the features of the consecutive vapor-liquid reactive distillation process for benzene chloride,on the basis of researching the distillation integrated structural parameters and manipulated parameters that established by economical steady-state optimum design,reasonably pairing of the controlled variables and manipulated variables for multiple loop control system is conducted by adopting relative steady-state gain array method,and three different control schemes (CS ~CS ) are designed respectively. The robustness of these1 3 three types of controlschemesunderdifferentfeedingflowrateandcompositiondisturbanceareanalyzedandcompared. Theresultof simulation indicatesthat by using the pairing structure mode,i.e. ,CS control scheme,in which the feed ratio control is adjusted by the temperature of 3 sensitive plate,and the quality of tower reactor is controlled by the heating value of reboiler,the closed loop system can reach better dynamic response performance and robustness. Keywords: Reactive distillation　 Automatic process control　 Multi-variable control　 B