hplc determination of paeoniflorin xie li xiao capsule（高效液相色谱法测定芍药苷谢立小胶囊）.docVIP

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hplc determination of paeoniflorin xie li xiao capsule（高效液相色谱法测定芍药苷谢立小胶囊）.doc

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hplc determination of paeoniflorin xie li xiao capsule（高效液相色谱法测定芍药苷谢立小胶囊）

HPLC determination of paeoniflorin Xie Li Xiao Capsule Abstract: Objective To establish the method for the determination of paeoniflorin Xie Li Xiao Capsule method column: Kromasil C18 column (4.6 mm × 250 mm, 5 μm, mobile phase: methanol-0.1% phosphoric acid solution (25:75, detection wavelength: 230 nm, flow rate: 1.0 mL · min-1 results paeoniflorin 0.484 ~ 2.422 μg (r = 0.999 9 linearity in the range of a good relationship, the regression equation is Y = 190 9276.923 1X - 4 265.72 (r = 0.999 9 ), average recoveries were 99.67% (RSD = 2.13% Conclusion The method is accurate and reliable, reproducible, and can be used for the paeoniflorin quality control Xie Li Xiao Capsule. Keywords: Xie Li Xiao Capsule, paeoniflorin, HPLC Xie Li Xiao Capsule wine Coptis, wine white peony root, prepared from 12 betel nut, Alisma, licorice, herbs processing, heat dampness, the effect of gas pain [1], used clinically in the large intestine damp heat caused by abdominal pain, diarrhea, poor stool, diarrhea sepsis embolism effect significantly the original standard content determination of the Coptis berberine component preparations, while the white peony nourishing yin, priorities and prescription to the drug that paeoniflorin the white peony active ingredients In the paeoniflorin preparations for the content determination, provide some reference for the perfect Xie Li Xiao Capsule quality control. 1 instrument and reagent 1.1 Instrument Agilent1100 high performance liquid chromatograph, a UV1100 UV spectrophotometer (Shanghai Tian Mei Scientific Instrument Co., Ltd., KQ-250 type ultrasonic cleaning device (Kunshan Ultrasonic Instrument Co., Ltd., AB135-S electronic balance (Mettler, Switzerland - Tropsch profitable company 1.2 reagent paeoniflorin reference substance (110736-200424 purchased from China Pharmaceutical and Biological Products, Xie Li Xiao Capsule (Yunnan Baiyao Group Co., Ltd. purchased from Qingdao Guofeng pharmacies, methanol, phosphate chromato