电子显微分析（章晓中）教学课件chapter12.pdfVIP

Extinction distance (消光距离） V cos g c F g In TEM,  is very mall, so cos  ~1. Hence V g Fc (5-2-5) g I I T D Example: Find the extinction distance  of silver at g reflection 200 under voltage of 100kV. V [Solution] g Fc g 3 3 3 (1) Find V : V =a =(4.089Å) =68.36Å c c (2) Find Fg: Silver is fcc structure and in a cell there are 4 atoms at positions of (000), (1/2 1/2 0), (1/2 0 1/2) and (0 1/2 1/2). n n   F f (e)e2ig rj f (e) exp 2i(hx  ky lz ) g j j j j j j 1 j 1 h k l k h l 2i( ) 2i ( ) 2i ( ) f (e)e2i0  f (e)e 2  f (e)e 2 f (e)e 2 For ghkl=200, F200=4f(e) where f(e) is the atomic scattering factor of electron. (3) Find f(e): we can find f(e) from the atomic scattering factor table （中文教科书附录C ）or the figure as shown if you know sin/. As sin 1   0.245  2d200 We find f(e) =5.41Å，so F =4f(e)=21.64Å