lcms联用技术分析金线莲中黄酮类和银线莲中核苷类活性成分及银线莲指纹图谱的研究-study on analysis of flavonoids in anoectochilus roxburghii, nucleoside active ingredients in anoectochilus roxburghii and fingerprint of anoectochilus roxburghii by lcms combined t.docxVIP
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lcms联用技术分析金线莲中黄酮类和银线莲中核苷类活性成分及银线莲指纹图谱的研究-study on analysis of flavonoids in anoectochilus roxburghii, nucleoside active ingredients in anoectochilus roxburghii and fingerprint of anoectochilus roxburghii by lcms combined t
目录目录................................................................................................................................1主要缩略词表................................................................................................................3中文摘要........................................................................................................................4ABSTRACT6前言................................................................................................................................8正文..............................................................................................................................12第一章LC-MS分析金线莲中4种黄酮类物质………………………………………...121引言........................................................................................................……..122材料和方法............................................................................................……..132.1主要仪器与试药................................................................................................132.2实验方法.................................................................................................143结果与讨论.......................................................................................................143.1色谱和提取条件的优选.........................................................................153.2标准溶液和金线莲提取物的HPLC-UV分析………………………..163.3LC-ESI(+)/MS鉴定金线莲中4种黄酮类物质……………………….173.4标准曲线的制备及线性关系的考察.....................................................253.5方法学考察.............................................................................................263.6样品测定.................................................................................................274结论...................................................................................................................27第二章LC-MS分析银线莲中6种核苷类物质......................................................281引言...................................................................................................................282材料和方法
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