螺旋通道型旋转床(RBHC)可控制备大孔容纳米纤维状拟薄水铝石-化学工艺专业毕业论文.docxVIP

IV IV and mass transfer is more quickly than normal gravity environment. Rotating Bed with Helix channels (RBHC), a novel multiphase contactor which can generate an acceleration 1~3 orders of magnitude larger than the gravitational acceleration on the earth, and liquid float velocity has been accelerated greatly, as well as the improvement of throughput and the reinforce of process of microcosmic mixing and material transmission, it has make the efficiency of volume per unit facility 1~2 higher in order of magnitude, it has been successfully applied to substances separation. Rotating Bed with Helix channels is also regarded as an ideal reactor for preparation of nano particles. Since it is able to greatly intensify micro mixing of fluids and the rate of mass transfer in a RBHC is much larger than that in a conventional packed bed. As a high-gravity reactor, RBHC is a better one, using the helix channels, it should not be packed with stuffing, that solved the problem of Rotating Packed Bed can be jammed easy. Rotating Bed With Helix Channels has been applied to the commercial production of nano calcium carbonate on the basis of above- mentioned research works. Therefore, RBHC is a very promising industrial platform for the production of inorganic nano powders. So this paper is using RBHC preparing nano fibrous pseudo boehmite (PB) with large pore volume and surface area. In this paper, based on the already studied in our group on preparation Pseudo boehmite with Rotating Bed With Helix Channels, systematically studied the high-gravity level, concentration of NaAlO2 solution, gas-liquid ratio, end pH of reaction and the technics of torrefaction effect on morphology and size of Pseudo boehmite. The result shows that, it can solve the mass-gathering in the drying process, and stability of high-gravity carbonization by azeotropic distillation method. It is known that, though the study of Surfactant and wet gel by azeotropic distillation method, the Surfactant can be reus