TA2工业纯钛高温组织演变研究-材料学专业论文.docxVIP

II II 形成界面不规则的 α 组织；从等轴 β 组织冷却时，β→α 相变分为晶界 α 和魏氏 α 的形核长大两个阶段，首先晶界 α 在 β 晶界处形核并长大连接 成薄膜状的晶界 α，随后魏氏 α 在晶界 α 上形核，并向以层片状集束的 形式向 β 相内长大，直到充满 β 晶粒时，β→α 转变结束，形成典型的魏 氏组织。 冷却速度对等轴 β 组织冷却过程中的 β→α 相变影响很大，冷却速度 越快，晶界 α 和魏氏 α 厚度越小，魏氏 α 伸长速度越快，相变速度越快。 对不同冷却速度下的晶界 α 的增宽、魏氏 α 的伸长和厚度，以及 β→α 相变动力学进行了定量统计，给出了 β→α 相变动力学经验公式。 关键词：工业纯钛，共焦激光扫描显微镜，显微组织，相变，动力学 III III MICROSTRUCTURE EVOLUTION OF TA2 COMMERCIAL PURE TITANIUM AT HIGH TEMPERATURE ABSTRACT TA2 commercial pure titanium has broad applications such as ship building and chemical industry for its outstanding corrosion resistance, good synthetic mechanical performance and excellent welding property. Its microstructure can be adjusted through heat treatment so as to get a good balance of strength, plasticity, and toughness. So it is very important to study the microstructure evolution behaviour at high temperature. The microstructure evolution behaviour of TA2 commercial pure titanium in heating, insulation and cooling processes were investigated by Confocal Laser Scanning Microscope, Optical Microscope, and Differential Scanning Calorimetry. During heating process, a part of curving α grain boundaries migrated and tend to be straighten. Short-time heating had little effect on α grain size. As the temperature was higher than Tα/α+β, several parallel “lense-shaped” β plates nucleated in the inside of an α grain and grew by consuming the surrounding α phase, being accompanied by “tent-shaped” surface reliefs. PAGE PAGE IV The β→α transformation ended as the temperature was higher than Tα+β/β. The parallel β plates in an α grain formed a cluster. The clusters devoured each other and formed equiaxed β grains. The kinetics of the β grain growth during heating and insulation processes was measured and fitted. Microstructures were different when cooled from different state. When cooled from α+β two-phase region, the microstructure restored to be equiaxed and the surface reliefs disappeared. When cooled from the state that α→β transformatio